4.7 Review

Nanoparticle and Nanostructure Synthesis and Controlled Growth Methods

Journal

NANOMATERIALS
Volume 12, Issue 18, Pages -

Publisher

MDPI
DOI: 10.3390/nano12183226

Keywords

nanomaterials dimensionality; synthesis approaches; reaction phase; mechanical synthesis; physical synthesis; chemical synthesis; physicochemical synthesis; biological synthesis; growth-controlled mechanisms

Funding

  1. Egypt-France Joint Driver (Imhotep Program) [43990SF]
  2. Irish Research Council [GOIPD/2020/340]
  3. Joint Egyptian Japanese Scientific Cooperation (JEJSC) [42811]
  4. Science and Engineering Research Board (SERB), Ministry of Science and Technology, India [CRG/2018/002135, BT/PR21547/NNT/28/1232/2017]
  5. Department of Biotechnology (DBT), Department of Science and Technology (DST), Ministry of Science and Technology, India [CRG/2018/002135, BT/PR21547/NNT/28/1232/2017]

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This article introduces the classification, fabrication, and functionalization techniques of nanomaterials, discusses synthesis methods and challenges.
Nanomaterials are materials with one or more nanoscale dimensions (internal or external) (i.e., 1 to 100 nm). The nanomaterial shape, size, porosity, surface chemistry, and composition are controlled at the nanoscale, and this offers interesting properties compared with bulk materials. This review describes how nanomaterials are classified, their fabrication, functionalization techniques, and growth-controlled mechanisms. First, the history of nanomaterials is summarized and then the different classification methods, based on their dimensionality (0-3D), composition (carbon, inorganic, organic, and hybrids), origin (natural, incidental, engineered, bioinspired), crystal phase (single phase, multiphase), and dispersion state (dispersed or aggregated), are presented. Then, the synthesis methods are discussed and classified in function of the starting material (bottom-up and top-down), reaction phase (gas, plasma, liquid, and solid), and nature of the dispersing forces (mechanical, physical, chemical, physicochemical, and biological). Finally, the challenges in synthesizing nanomaterials for research and commercial use are highlighted.

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