Characterization of Wear Properties of Pure Nickel Modified by Ni-Cr Composite and CaF2 Solid Lubricant Addition

Nickel composites doped by chromium and calcium fluoride were produced by powder metallurgy. The friction coefficient of the samples containing 20% of the CaF2 was lower at elevated temperatures (600 degrees C) than the friction coefficient for the Ni-50%NiCr(80/20) composite (0.14 vs. 0.20). Sample surfaces were analyzed by the scanning electron microscope (SEM). EDS analysis proved tribofilm formation on the surface of the sample with CaF2 addition. A laser confocal microscope (LCM) was used to investigate the surface condition of the counter-sample after wear tests. The presence of the tribofilm reduced the wear of the frictional pair, and because of that the wear tracks were smooth. Tribofilm limited the abrasive wear and ploughing. Therefore, the tribofilm protected the sample and counter-sample from wear.

Automated summary

Nickel composites doped with chromium and calcium fluoride were synthesized using powder metallurgy. The friction coefficient of samples with 20% CaF2 was lower at high temperatures (600 degrees C) compared to a Ni-50%NiCr(80/20) composite. Analysis of the sample surfaces revealed the formation of a tribofilm, and wear tests showed that the presence of the tribofilm reduced wear in the frictional pair.