Journal
CARBOHYDRATE RESEARCH
Volume 401, Issue -, Pages 109-114Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.carres.2014.09.010
Keywords
Oligomannose; Glycosylation; One-pot; Thioglycoside
Funding
- Major State Basic Research Development Program of China (973 Program) [2012CB822102]
- National Natural Science Foundation of China [21172135, 21372145]
- Excellent Young Scientist Research Award Fund of Shandong Province [2012BSE27170]
- Development Fund for Collaborative Innovation Center of Glycoscience of Shandong University
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An expeditious three-component, one-pot sequential glycosylation protocol has been developed for the preparation of 3,6-branched unsymmetrical mannopentaose (Man5), employing a mannose trisaccharide donor, a mannose monosaccharide donor and a mannose monosaccharide acceptor. The high efficiency of this one-pot procedure was demonstrated by comparison study with a stepwise synthesis using the same three building blocks. (C) 2014 Elsevier Ltd. All rights reserved.
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