4.7 Article

Microwave radiation technique for the isolation of Sunn Hemp natural fiber in the application of material processing

Journal

JOURNAL OF NON-CRYSTALLINE SOLIDS
Volume 591, Issue -, Pages -

Publisher

ELSEVIER
DOI: 10.1016/j.jnoncrysol.2022.121706

Keywords

Natural fiber; Physical treatment; Composite; Interface; Mechanical properties

Funding

  1. Ministry of Human Resource and Development (MHRD), India
  2. Ministry of Human Resource and Development (MHRD) , India, under the indigenous fellowship scheme

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This study conducted experimental research on Sunn Hemp fiber and its reinforced composite, focusing on the structural and physical properties of the fiber and composite. The research found that the treated fiber showed increased crystallinity and crystallite size, while its basic crystallinity remained unchanged. The morphology of the treated fiber exhibited fibrillation and rough surfaces, but a higher degree of treatment made the fiber more brittle and carbonized. Changes in hydrophilicity and crosslinking density affected the flexural and tensile properties of the treated composites.
Experimental works have been done on Sunn Hemp fiber and its reinforced composite to investigate various properties. Sunn Hemp fiber is modified physically by a multimode microwave oven (2.45 Hz) at the power of 160W-800W with 120W with varying time from 2 to 10 min with 4 min of interval. The fiber and composite properties are characterized structurally and physically. An increase in crystallinity and crystallite size in treated fiber is observed in X-Ray Diffraction (XRD) study, where Fourier Transmission Infrared (FTIR) shows no change in basic crystallinity in fiber. Morphology of treated fiber shows fibrillation and rough surface, but a higher treatment makes the fiber brittle and carbonized. Change in hydrophilicity from contact angle study and crosslinking density from equilibrium swelling theory affects the flexural and tensile properties of treated composites.

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