4.7 Article

Using real-time data analysis to conduct next-generation synchrotron fatigue studies

Journal

INTERNATIONAL JOURNAL OF FATIGUE
Volume 164, Issue -, Pages -

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.ijfatigue.2022.107113

Keywords

Low cycle fatigue; Synchrotron X-ray diffraction; Mathematical analysis; Micromechanics

Funding

  1. U.S. Department of Energy, Basic Energy Sciences, USA, Division of Materials Sciences and Engineering, USA [DE-SC0018901]
  2. National Science Foundation, USA [DMR-1829070]

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This study presents a framework for real-time monitoring of the evolution of a deforming polycrystal using principal component analysis (PCA) applied to X-ray diffraction image data. The researchers discovered correlations between PCA of the diffraction data and the physical processes in the polycrystal, which is significant for understanding fatigue failure processes.
Next-generation experimental techniques, like high energy X-ray diffraction microscopy (HEDM), usher in new opportunities to collect the grain-scale data necessary for understanding the evolving processes that drive fatigue failure. In this study, we present a framework for monitoring the evolution of a deforming polycrystal, in real-time, by applying principal component analysis (PCA) to raw X-ray diffraction image data. We applied this framework to inform in-situ HEDM measurements of a cyclically loaded Inconel-718 superalloy. We discovered correlations between PCA of the diffraction data and the physical processes in the polycrystal. Lastly, we discuss extending this framework in future HEDM fatigue studies.

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