Journal
CARBOHYDRATE POLYMERS
Volume 126, Issue -, Pages 9-16Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.carbpol.2015.03.021
Keywords
Cassava starch; Acetylation; Nanoparticles; Thermoplastic starch; Mechanical properties; Biodegradable films
Categories
Funding
- Fundacao Araucaria (Brazil)
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This paper reports the use of acetylated starch nanoparticles (NPAac) as reinforcement in thermoplastic starch films. NPAac with an average size of approximately 500 nm were obtained by nanoprecipitation. Fourier transform infrared (FTIR) and thermogravimetric analysis (TGA) indicated that NPAac are more thermally stable and essentially amorphous when compared with acetylated starch. Thermoplastic starch films with different proportions of NPAac (0.5, 1.0, 1.5, 10.0%, w/w) were obtained and characterized by scanning electron microscopy (SEM), water vapor permeability (WVP), adsorption isotherms, TGA and mechanical tests. The inclusion of reinforcement caused changes in film properties: WVP was lowered by 41% for film with 1.5% (w/w) of NPAac and moisture adsorption by 33% for film with 10% (w/w) of NPAac; and the Young's modulus and thermal stability were increased by 162% and 15%, respectively, for film with 0.5% (w/w) of NPAac compared to the starch film without the addition of NPAac. (C) 2015 Elsevier Ltd. All rights reserved.
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