4.5 Article

Production of ethyl lactate by reactive dividing wall column using analysis of the statics

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ELSEVIER SCIENCE SA
DOI: 10.1016/j.cep.2022.109150

Keywords

Reactive distillation; Analysis of the statics; Reactive dividing wall column distillation; Esterification of lactic acid

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Sustainable development in separation-reaction processes aims to improve energy efficiency and reduce pollutants. The analysis of the statistics methodology enables the development of optimal qualitative technological schemes with minimal data, allowing for intensified separation and higher conversion rates.
The sustainable development in separation-reaction processes involves a higher energy efficiency and pollutant reduction. The main interest of the analysis of the statics methodology is developed the optimal qualitative technological scheme with minimal data, the physicochemical information of the system, and the stoichiometry of the reaction. This results in a feasible intensified scheme flowsheet and a reactive distillation column (RD) that are then implemented in a reactive dividing wall column (RDWC) distillation to produce ethyl lactate from the esterification of lactic acid with ethanol. The RDWC configuration showed a reduction of 38% in the save net duty and an increase of 13% in the conversion compared with a conventional direct sequence. The analysis of the statics method presents an alternative in the design stage in a complex column, allowing for a feasible operation in different degrees of process intensification.

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