Journal
JOURNAL OF FLUORINE CHEMISTRY
Volume 185, Issue -, Pages 168-172Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jfluchem.2016.03.006
Keywords
2-Mercaptobenzimidazole; Chlorotrifluoroethylene; Hexafluoropropene; Single crystal X-ray diffraction analysis
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The unusual cyclization mode of 2-mercaptobenzimidazole with chlorotrifluoroethylene and hexafluoropropene has been found. Such unexpected products as 2-chloro-2,3,3-trifluoro-2,3-dihydrobenzimidazo[4,513]thiazole-1,3 and 2-trifluoromethy1-2,3,3-trifluoro-2,3-dihydrobenzimidazo[4,5b]thiazole-1,3 were isolated. The structures of obtained compounds were supported by single crystal X-ray diffraction analysis and the possible reaction route was proposed. (C) 2016 Elsevier B.V. All rights reserved.
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