Journal
CHEMISTRYSELECT
Volume 7, Issue 26, Pages -Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/slct.202200914
Keywords
acylation; carbonylation; Mo(CO)(6); nickel
Categories
Funding
- Natural Science Foundation in Henan Province Department of Education [21A150016]
- Innovative Funds Plan of Henan University of Technology [2020ZKCJ29]
- Henan Province Key Research and Development of Science and Technology [212102310332]
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A nickel-catalyzed molybdenum-promoted carbonylative synthesis method has been developed for the synthesis of aryl thioesters without the presence of CO gas. This method uses Mo(CO)(6) as a solid CO source to obtain a variety of thioesters in moderate yields without the use of expensive metals such as palladium.
A nickel-catalyzed molybdenum-promoted carbonylative synthesis of thioesters between aryl iodides and dialkyl disulfides has been developed. This method provides a novel and practical route to aryl thioesters under CO-gas-free conditions. Using Mo(CO)(6) as a solid CO source, many thioesters were obtained in moderate yields without expensive metals such as palladium.
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