4.7 Article

Recrystallization and grain growth kinetics of IN718 manufactured by laser powder bed fusion

Journal

JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
Volume 19, Issue -, Pages 4242-4257

Publisher

ELSEVIER
DOI: 10.1016/j.jmrt.2022.06.157

Keywords

IN718; Laser powder bed fusion; Solution heat treatment; Microstructure; Texture; Recrystallization; Electron backscatter diffraction

Funding

  1. Science Foundation Ireland (SFI) [16/RC/3872]
  2. European Regional Development Fund

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The recrystallization and grain growth behavior of IN718 alloy manufactured by laser powder bed fusion were studied. The texture evolution of the samples under different temperatures and holding times was investigated, and it was found that the formation of recrystallization nuclei was related to high defect density regions, while the presence of non-coherent precipitates limited the growth of recrystallized grains.
The recrystallization and grain growth behaviour of IN718 alloy additively manufactured by laser powder bed fusion (L-PBF) is presented herein. The effects of three different temperatures (1050, 1150 and 1250 degrees C) and holding times (15, 45 and 90 min) were investigated. The texture evolution of the samples was recorded via electron backscatter diffraction (EBSD). The as-built sample is composed of bowl-shaped melt pools, a chessboard-like grain pattern and has a cube texture {100}<001>. Recrystallized grains were observed in the samples treated at 1150 degrees C for 15 min, as well as the samples treated for longer periods and at higher temperatures. Recrystallization was observed to start from high dislocation density regions, including the overlapping melt pools and the borders of the chessboard-like pattern. The initial cube texture transforms into a first-generation cube-twin texture {122}<212> via a twinning-assisted recrystallization mechanism. Then, those recrystallization nuclei sweep through the high defect density matrix; during which almost no new twins are formed. The samples treated at 1250 degrees C are almost completely recrystallized, which forms a weaker cube texture and a stronger P-orientation {011}<112>. However, the growth of recrystallized grains is very limited due to the presence of non-coherent precipitates. (C) 2022 The Author(s). Published by Elsevier B.V.

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