Journal
NANOMATERIALS
Volume 12, Issue 13, Pages -Publisher
MDPI
DOI: 10.3390/nano12132268
Keywords
single crystal; crystal structure; nanoparticle; phosphazene; X-ray diffraction
Categories
Funding
- Russian Science Foundation [22-43-02056]
Ask authors/readers for more resources
The synthesized compound was characterized using NMR spectroscopy and mass spectrometry, and the crystal structure was determined by X-ray diffraction study.
The synthesized compound was characterized by P-31, C-13, and H-1 NMR spectroscopy and MALDI-TOF mass spectroscopy. According to DSC data, the compound was initially crystalline, but the crystal structure was defective. The crystals suitable for X-ray diffraction study were prepared by slow precipitation of the compound from a solution by a vapor of another solvent. A study of the single crystal obtained in this way demonstrated that the phosphazene ring has a flattened chair conformation. It was found that the sphere circumscribed around the compound molecule has a diameter of 2.382 nm.
Authors
I am an author on this paper
Click your name to claim this paper and add it to your profile.
Reviews
Recommended
No Data Available