4.5 Article

Microstructural Evolution and Stability of Coarse-Grained S31254 Super Austenitic Stainless Steel during Hot Deformation

Journal

METALS
Volume 12, Issue 8, Pages -

Publisher

MDPI
DOI: 10.3390/met12081319

Keywords

super austenitic stainless steel; coarse-grained austenite; constitutive model; processing map; hot tensile; dynamic recrystallization

Funding

  1. Fundamental Research Program of Shanxi Province [20210302124044]

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The stress-strain response and microstructural evolution of coarse-grained S31254 super austenitic stainless steel were investigated. The results showed that temperature and strain rate significantly influenced the energy required for plastic deformation and deformation mechanism. A constitutive equation and processing maps were established, and optimal processing parameters were clarified.
The ingot of S31254 super austenitic stainless steel (SASS) was annealed at 1220 degrees C for 70 h to eliminate the segregation of Mo element, and the grain size grows to the level of millimeter. The stress-strain response and microstructural evolution of coarse-grained S31254 SASS were investigated by hot compression tests in the temperature range of 950-1250 degrees C and strain rate range of 0.001-10 s(-1). The results showed that the energy required for plastic deformation improved with the increase of strain rate and the decrease of deformation temperature. The hot deformation activation energy was calculated to be 542.91 kJ center dot mol(-1) through the regression analysis of hyperbolic-sine function, and the constitutive equation was established. Processing maps were constructed, and two optimal hot working parameters ranges were clarified. Due to the low fraction of grain boundaries, the main deformation mechanism of coarse-grained S31254 SASS was dynamic recovery. However, when the deformation temperature improved to 1250 degrees C, recrystallized grains began to nucleate and grow along with the band-like structure within the austenitic grains. When the deformation temperature is 950-1150 degrees C, the microstructural stability of S31254 SASS under tension stress was excellent. However, when the temperature and the strain rate were 1250 degrees C and 0.5 s(-1) respectively, the microstructural stability deteriorated resulting from the formation of delta-ferrite phase and local melting of austenitic grain boundaries.

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