4.7 Review

In Situ Thermoset Cure Sensing: A Review of Correlation Methods

Journal

POLYMERS
Volume 14, Issue 15, Pages -

Publisher

MDPI
DOI: 10.3390/polym14152978

Keywords

composite manufacturing; thermosetting polymers; cure behaviour; process monitoring; in situ cure monitoring; sensors

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This paper provides a critical review of different data collection and cure state correlation methods for thermoset polymer composites. It includes details of sensor configurations, governing equations, data verification techniques, and discusses qualitative and quantitative analysis methods. The capability and limitations of these methods are analyzed in identifying cure state information for the materials under investigation.
Thermoset polymer composites have increased in use across multiple industries, with recent applications consisting of high-complexity and large-scale parts. As applications expand, the emphasis on accurate process-monitoring techniques has increased, with a variety of in situ cure-monitoring sensors being investigated by various research teams. To date, a wide range of data analysis techniques have been used to correlate data collected from thermocouple, dielectric, ultrasonic, and fibre-optic sensors to information on the material cure state. The methods used in existing publications have not been explicitly differentiated between, nor have they been directly compared. This paper provides a critical review of the different data collection and cure state correlation methods for these sensor types. The review includes details of the relevant sensor configurations and governing equations, material combinations, data verification techniques, identified potential research gaps, and areas of improvement. A wide range of both qualitative and quantitative analysis methods are discussed for each sensing technology. Critical analysis is provided on the capability and limitations of these methods to directly identify cure state information for the materials under investigation. This paper aims to provide the reader with sufficient background on available analysis techniques to assist in selecting the most appropriate method for the application.

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