4.1 Article

The crystal structure of dimethylammonium 8-[(7,9-dioxo-6,10-dioxaspiro[4.5]decan-8-ylidene)methyl]-9-oxo-6,10-dioxaspiro[4.5] dec-7-en-7-olate, C19H25NO8

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WALTER DE GRUYTER GMBH
DOI: 10.1515/ncrs-2022-0200

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Funding

  1. National Natural Science Foundation of China [22108208]
  2. Foundation of State Key Laboratory of High-Efficiency Utilization of Coal and Green Chemical Engineering [2021-K02]
  3. National Innovation and Entrepreneurship Training Program for College Students [202111067020]

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This is the structural parameter of a C19H25NO8 compound. It belongs to the monoclinic system with space group P2(1)/n. The cell parameters of the compound are a = 10.149(2) angstrom, b = 12.338(3) angstrom, c = 15.898(3) angstrom, β = 97.58(3) degrees, and the volume is 1973.2(7) angstrom cubed. The cell contains 4 molecules. The fitting parameters for the structure are R-gt(F) = 0.0581 and wR(ref)(F-2) = 0.1842. The measurement temperature is 293(2) K.
C19H25NO8, monoclinic, P2(1)/n (no. 14), a = 10.149(2) angstrom, b = 12.338(3) angstrom, c = 15.898(3) angstrom, beta = 97.58(3)degrees, V = 1973.2(7) angstrom(3), Z = 4, R-gt(F) = 0.0581, wR(ref) (F-2) = 0.1842, T = 293(2) K.

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