Journal
SEPARATION AND PURIFICATION REVIEWS
Volume 52, Issue 3, Pages 262-282Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/15422119.2022.2094274
Keywords
Extraction and microextraction; matrix solid-phase dispersion; natural products; novel adsorbent; novel elution solvent; sample preparation
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Matrix solid phase dispersion (MSPD) is a rapid and flexible sample pretreatment method that allows efficient extraction of active compounds from natural products. This review systematically discusses the latest developments and applications of MSPD microextraction techniques.
Matrix solid phase dispersion (MSPD) is a rapid and flexible sample pretreatment method that accomplishes sample disruption, extraction, filtering and purification in one step and is especially suitable for solid, semisolid and viscous samples. More than 30 years have elapsed since it was first proposed, and there are many published reviews. However, there is no review on the use of MSPD to extract active compounds from natural products. In this review, the latest developments from 2015-2021 in MSPD microextraction techniques, including sorbents, elution solvents and assisted MSPD extraction, along with their applications in natural products, are systematically discussed and classified according to the structure of the active constituents, which mainly refer to phenolic acids, flavonoids, alkaloids, anthraquinones and terpenes.
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