Journal
POLYHEDRON
Volume 222, Issue -, Pages -Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.poly.2022.115938
Keywords
Cucurbit[7]uril; 1-[4-(dimethylamino)phenyl]-ethanone; Hostguest complex; Structure
Categories
Funding
- Innovation Program for High-level Talents of Guizhou Province [2016-5657]
- Science and Technology Fund of Guizhou Province [[2020] 1Y051]
- EPSRC [EP/R023816/1]
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In this work, we investigated the interaction between Q[7] and DAPE using various techniques, and found the formation of a 1:1 complex. Additionally, we reported the molecular structure of the complex [(Q[7]@DAPE)Ca(H2O)(3)](2)(CdCl4)(2)center dot 31(H2O).
In the work, we have studied the interaction of cucurbit[7]uril (Q[7]) with 1-[4-(dimethylamino)phenyl]-ethanone (DAPE) using a variety of techiniques including H-1 NMR spectroscopy, UV-vis adsorption and fluorescence spectroscopies, Isothermal titration calorimetry and single crystal X-ray diffraction. Results revealed the formation of a 1:1 complex, whilst the molecular structure of the species [(Q[7]@DAPE)Ca(H2O)(3)](2)(CdCl4)(2)center dot 31(H2O) is reported.
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