Journal
ORGANIC LETTERS
Volume 24, Issue 24, Pages 4409-4414Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.2c01637
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Funding
- National Natural Science Foundation of China [22165026]
- Open Fund of Guangdong Provincial Key Laboratory of Luminescence from Molecular Aggregates (South China University of Technology) [2019B030301003]
- Key Laboratory of Eco-functional Polymer Materials of the Ministry of Education (Northwest Normal University)
- Ministry of Education Scholars Innovation Team [IRT 1177]
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In this study, O-18-labeled aromatic aldehydes (3a-3x) were successfully obtained with high total yields (52-72%) and sufficient O-18 abundance (90.90-96.09%) using the reversed Knoevenagel reaction. This work is of great importance for the labeling and research of organic substances.
Obtaining O-18-labeled organic substances is of great research importance and also an extremely challenging work. In this work, depending on the reversed Knoevenagel reaction, O-18-labeled aromatic aldehydes (3a-3x) are successfully obtained with high total yields (52-72%) and sufficient O-18 abundance (90.90-96.09%).
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