Journal
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
Volume 42, Issue 8, Pages 3415-3426Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.jeurceramsoc.2022.02.047
Keywords
MAX phase; Ti3SiC2; Diffusion; Bonding; Au; Nuclear fuel cladding
Categories
Funding
- National Natural Science Foundation of China [51775142, 51805113]
- China Postdoctoral Science Foundation [2020T130143, 2018M631923]
- Fundamental Research Funds for the Central Universities [FRFCU5710050920]
- National Key R&D Program of China [2019YFA0705201]
- Heilongjiang Touyan Team [XNAUEA 5640202520]
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A reliable diffusion bonding of Ti3Si(Al)C-2 ceramic is achieved by using Au foil as an interlayer at a lower temperature and shorter time. This method significantly decreases the bonding temperature by about 150 degrees Celsius compared to the lowest temperature reported in current research, and achieves a higher shear strength at 650 degrees Celsius.
Herein, a reliable diffusion bonding of Ti3Si(Al)C-2 ceramic is achieved by applying Au foil as an interlayer at 650 degrees C for 30 min with an axial pressure of 20 MPa. This novel method significantly decreases the bonding temperature, which is about 150 degrees C lower than the lowest bonding temperature from current research to the best of our knowledge. Maximum shear strength of 58 MPa is achieved at 650 degrees C among the bonding temperature range of 600 degrees C similar to 800 degrees C. The microstructure evolution mechanism and the relationship between microstructure and mechanical property are discussed. The facile mutual diffusion of Au with de-intercalated Al and Si from Ti3Si(Al)C-2 is considered critical in achieving sound interfacial bonding.
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