Journal
JOURNAL OF COORDINATION CHEMISTRY
Volume 69, Issue 16, Pages 2493-2499Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/00958972.2016.1186801
Keywords
Copper complex; 5-methylsalicylaldehyde; 2,2 '-bipyridine; crystal structure; urease inhibition
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Funding
- Natural Science Foundation of Liaoning Province [2015020673]
- Program for Liaoning Excellent Talents in University [LR2014032]
- Undergraduate Training Program for Innovation and Entrepreneurship of Liaoning Province [201510165079]
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A dicyanoamide-bridged polymeric copper(I/II) complex, [Cu-II(sal)(bipy)Cu-I(dca)(2)](n), was prepared by reaction of 5-methylchlorosalicylaldehyde (Hsal), 2,2-bipyridine (bipy), sodium dicyanoamide (Nadca), and copper perchlorate in methanol. The complex was characterized by elemental analyses, infrared and electronic spectroscopy, and single-crystal X-ray determination. Cu-II has a square pyramidal coordination, and Cu-I has triangular coordination. The complex showed high urease inhibitory activity with IC50 value of 0.16 +/- 0.23M. [GRAPHICS] .
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