Journal
JOURNAL OF CLUSTER SCIENCE
Volume 28, Issue 3, Pages 949-962Publisher
SPRINGER/PLENUM PUBLISHERS
DOI: 10.1007/s10876-016-1079-7
Keywords
Metal organic frameworks; Post-synthetic modification; Heterogeneous catalysis; Nickel
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Funding
- Research Council of University of Guilan
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Nickel-pyridylimine complex was incorporated into (Cr)NH2-MIL-101 through condensation of 2-pyridine carboxaldehyde and NiCl2 in presence of (Cr)NH2-MIL-101-MOF in a one pot method. The prepared catalyst was characterized by XRD, FTIR, SEM, TEM and NMR methods. The obtained catalyst demonstrates an appropriate pattern for a post-synthetic covalent modification with catalytic active sites. This heterogeneous catalyst showed efficiency in the epoxidation reaction of chalcones and bischalcones, and exhibited appropriate recyclability, rather short reaction times and high yields.
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