4.7 Article

Superplasticity of a friction stir processed overaged WE54 magnesium alloy

Journal

JOURNAL OF MAGNESIUM AND ALLOYS
Volume 10, Issue 11, Pages 3156-3166

Publisher

KEAI PUBLISHING LTD
DOI: 10.1016/j.jma.2022.02.008

Keywords

WE54 magnesium alloy; Friction stir processing; Processing severity; Superplasticity; Grain boundary sliding; Solutes

Funding

  1. MINECO (Spain) [MAT2015-68919-C3-1-R]
  2. CENIM, CSIC
  3. MINECO [BES2013-063963]

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Through friction stir processing, the WE54 magnesium alloy obtained superplasticity at high temperatures, with grain sizes less than 1μm and a tensile superplastic elongation of 756%, attributed to the grain boundary sliding mechanism (GBS).
The coarse-grained WE54 magnesium alloy was heat treated in order to have minimum hardness minimizing the effects of precipitates and solid solution. Friction stir processing (FSP) was applied in severe conditions to obtain fine, equiaxed and highly misoriented grains, with grain sizes even less than 1 mu m. The high severity of processing demonstrated to have a strong impact in the microstructure. Consequently, the processed materials exhibited excellent superplasticity at the high strain rate 10(-2) s(-1), and temperatures between 300 and 400 degrees C. The maximum tensile superplastic elongation of 756% was achieved at 400 degrees C thanks to the operation of grain boundary sliding mechanism (GBS). Besides the new data obtained through tensile testing, the paper deals with a transcendental question regarding the large differences in strain rate values at a given stress in the superplastic regime at maximum elongation compared to other magnesium-based alloys. With this is mind, 19 magnesium alloys from 22 different investigations were analyzed to give some light to this behavior that never was treated before. It is proposed that this behavior has to be attributed to the accommodation process, necessary for GBS to occur, which is hindered by reinforcing solutes. (c) 2022 Chongqing University. Publishing services provided by Elsevier B.V. on behalf of KeAi Communications Co. Ltd. This is an open access article under the CC BY-NC-ND license ( http://creativecommons.org/licenses/by-nc-nd/4.0/ ) Peer review under responsibility of Chongqing University

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