4.6 Article

The Influence of Sintering Temperature on the Pore Structure of an Alkali-Activated Kaolin-Based Geopolymer Ceramic

Journal

MATERIALS
Volume 15, Issue 7, Pages -

Publisher

MDPI
DOI: 10.3390/ma15072667

Keywords

geopolymer; pore; tomography imaging; sintering

Funding

  1. Ministry of Education Malaysia [JPT.S (BPKI)2000/016/018/019(29)]
  2. TUIASI's internal grants program (GI_PUBLICATIONS/2021) - Romanian Government
  3. Ministry of Higher Education Malaysia
  4. UK Department of Business, Energy and Industrial Strategy (BEIS)

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Geopolymer materials are low-carbon construction materials. Alkali-activated kaolin, a type of geopolymer material, is a viable alternative for high-strength ceramics. This study analyzed the sintering process and pore structure of alkali-activated kaolin, revealing the effects of different sintering temperatures on pore distribution.
Geopolymer materials are used as construction materials due to their lower carbon dioxide (CO2) emissions compared with conventional cementitious materials. An example of a geopolymer material is alkali-activated kaolin, which is a viable alternative for producing high-strength ceramics. Producing high-performing kaolin ceramics using the conventional method requires a high processing temperature (over 1200 degrees C). However, properties such as pore size and distribution are affected at high sintering temperatures. Therefore, knowledge regarding the sintering process and related pore structures on alkali-activated kaolin geopolymer ceramic is crucial for optimizing the properties of the aforementioned materials. Pore size was analyzed using neutron tomography, while pore distribution was observed using synchrotron micro-XRF. This study elucidated the pore structure of alkali-activated kaolin at various sintering temperatures. The experiments showed the presence of open pores and closed pores in alkali-activated kaolin geopolymer ceramic samples. The distributions of the main elements within the geopolymer ceramic edifice were found with Si and Al maps, allowing for the identification of the kaolin geopolymer. The results also confirmed that increasing the sintering temperature to 1100 degrees C resulted in the alkali-activated kaolin geopolymer ceramic samples having large pores, with an average size of similar to 80 mu m(3) and a layered porosity distribution.

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