4.1 Article

The crystal structure of 1,2-bis(pyridinium-4-yl)ethane diperchlorate, C12H14N2•2ClO4 - a second polymorph

Journal

Publisher

WALTER DE GRUYTER GMBH
DOI: 10.1515/ncrs-2022-0190

Keywords

2164314

Funding

  1. Analytical and Testing Centre in Beijing Institute of Technology
  2. New Teachers' Basic Scientific Research Ability Improvement Project in China University of Geosciences [2-9-2021-008]

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C12H14N2·2ClO(4) is monoclinic with the space group P2(1)/c (no. 14). The crystal parameters are: a = 5.3170(4) Å, b = 12.8711(8) Å, c = 11.6788(7) Å, β = 100.888(2) degrees, and the volume is 784.86(9) Å^3.
C12H14N2 center dot 2ClO(4), monoclinic, P2(1)/c (no. 14), a = 5.3170(4) angstrom, b = 12.8711(8) angstrom, c = 11.6788(7) angstrom, beta = 100.888(2)degrees, V = 784.86(9) angstrom(3), Z = 2, R ( gt )(F) = 0.0434, wR ( ref )(F (2)) = 0.1211, T = 298 K.

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