Journal
RUSSIAN JOURNAL OF GENERAL CHEMISTRY
Volume 92, Issue 2, Pages 272-275Publisher
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S1070363222020189
Keywords
niobium diboride nanoparticles; niobium pentachloride; sodium borohydride; ionic melts of alkali metal halides; autoclave
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Funding
- Ministry of Science and Higher Education of the Russian Federation [.....-.19-119061890019-5]
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Near-spherical niobium diboride nanoparticles with an average diameter of about 17 nm were synthesized by reacting NbCl5 with NaBH4 in ionic melts of alkali metal halides at 1073 K under an argon pressure of 4 MPa for 15 hours in an autoclave.
Near-spherical niobium diboride nanoparticles with an average diameter of similar to 17 nm, crystallizing in the hexagonal system and belonging to the space group P6/mmm, were obtained by reacting NbCl5 with NaBH4 in ionic melts of alkali metal halides at 1073 K under an argon pressure of 4 MPa for 15 h in an autoclave.
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