☆ 4.5 Review

Recent advances in NMR spectroscopy of ionic liquids

PROGRESS IN NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY (2022)

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Article Chemistry, Physical

Polar/apolar domains' dynamics in alkylimidazolium ionic liquids unveiled by the dual receiver NMR 1H and 19F relaxation experiment

Maria Enrica Di Pietro et al.

Summary: The spin-lattice relaxation times of both cation and anion forming ionic liquid materials were simultaneously measured using the dual receiver H-1/F-19 inversion-recovery NMR method. Experimental data analysis showed that the overall dynamic behavior of ionic liquids is influenced by the length of the alkyl chain and the capability of the anion to disrupt or stabilize the apolar domain structure.

JOURNAL OF MOLECULAR LIQUIDS (2021)

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Article Chemistry, Multidisciplinary

Low Temperature Activation of Tellurium and Resource-Efficient Synthesis of AuTe2and Ag2Te in Ionic Liquids

Matthias A. Grasser et al.

Summary: The low temperature syntheses of AuTe(2) and Ag2Te starting from the elements were investigated in ionic liquids, revealing [P-66614]Cl as the most promising candidate for single phase AuTe(2) synthesis at 200°C, while Ag2Te could be obtained by reducing the temperature in the flask to 60°C. Additionally, using [P-66614]Cl in dichloromethane or a planetary ball mill resulted in quantitative yield even at room temperature. Further experiments uncovered a reaction mechanism involving alkylphosphanes in [P-66614]Cl activating tellurium and forming soluble phosphane tellurides.

CHEMISTRYOPEN (2021)

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Article Chemistry, Multidisciplinary

Metal Assisted Synthesis of Cationic Sulfidobismuth Cubanes in Ionic Liquids

Maximilian Knies et al.

Summary: By dissolving Bi(2)S(3) in ionic liquids containing AuCl/PtCl(2) or AgCl and annealing at certain temperatures, orange crystals of [BMIm](Bi4S4)[AlCl4](5) and Ag(Bi7S8)[S(AlCl3)(3)](2)[AlCl4](2) were successfully precipitated. The involvement of metal cations was found essential for the formation of these crystals, which exhibited complex structures with significant intercalation effects.

CHEMISTRYOPEN (2021)

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Article Food Science & Technology

Fast field cycling NMR relaxometry as a tool to monitor Parmigiano Reggiano cheese ripening

Pellegrino Conte et al.

Summary: This study investigated the chemical-physical characteristics of Parmigiano Reggiano cheese aged at different time points and found that aging led to decomposition of organic components, increase in long chain fatty acids, and changes in water activity. Fast field cycling NMR relaxometry was identified as a promising technique for monitoring chemical physical changes during Parmigiano Reggiano cheese ripening.

FOOD RESEARCH INTERNATIONAL (2021)

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Article Chemistry, Physical

Role of cationic head-group in cytotoxicity of ionic liquids: Probing changes in bilayer architecture using solid-state NMR spectroscopy

Navleen Kaur et al.

Summary: The effect of cationic head-group of ionic liquid on the structure and dynamics of phospholipid bilayer was studied using six different ionic liquids. Different cations showed varying impact on the orientation and disorder in lipid head-group, as well as lipid chain dynamics in the bilayer. These results suggest a correlation between structural changes induced by ionic liquid head-group and membrane disruption.

JOURNAL OF COLLOID AND INTERFACE SCIENCE (2021)

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Article Biochemical Research Methods

Field-cycling NMR and DNP - A friendship with benefits

Bulat Gizatullin et al.

Summary: Field-cycling relaxometry is an inherently insensitive technique due to construction compromise for a fast-switching, low-inductance magnet; Dynamic Nuclear Polarization (DNP) has the potential to enhance magnetization and provide selectivity, but requires stable radicals introduction.

JOURNAL OF MAGNETIC RESONANCE (2021)

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Article Chemistry, Physical

Rotational correlation times, diffusion coefficients and quadrupolar peaks of the protic ionic liquid ethylammonium nitrate by means of 1H fast field cycling NMR relaxometry

Viviane Overbeck et al.

Summary: The protic ionic liquid ethylammonium nitrate (EAN) is characterized by hydrogen bonding similar to water. Through Fast Field Cycling NMR relaxometry, rotational correlation times and translational diffusion coefficients of EAN were successfully measured and analyzed as functions of temperature and frequency. Additionally, quadrupole relaxation enhancement was observed in EAN, a phenomenon rarely seen in liquids.

JOURNAL OF MOLECULAR LIQUIDS (2021)

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Article Chemistry, Physical

Intra- and inter-molecular interactions in choline-based ionic liquids studied by 1D and 2D NMR

Emmanouil Veroutis et al.

Summary: Choline acetate and choline trifluoroacetate mixed with water participate in a strong local hydrogen bond network, with no evidence of large ion clusters. Trifluoroacetate shows weaker association effects than acetate due to its higher anion acidity. Temperature dependent measurements reveal collective reorientation of cations, anions, and water molecules even at room temperature.

JOURNAL OF MOLECULAR LIQUIDS (2021)

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Article Chemistry, Physical

Ionic Liquid Aggregation Mechanism for Nanoparticle Synthesis

Kristin Bryant et al.

Summary: The use of silylamine reversible ionic liquids for nanoparticle synthesis allows for size control without the need for additional stabilizing agents. The mechanism of nanoparticle formation involves a switchable aggregation mechanism rather than a reverse micelle mechanism. The addition of water affects the aggregation behavior of the ionic liquid molecules but does not impact nanoparticle size during reduction.

JOURNAL OF PHYSICAL CHEMISTRY B (2021)

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Article Chemistry, Physical

Chelating Additives Reversing the Lithium Migration Direction in Ionic Liquid Electrolytes

Florian Ackermann et al.

Summary: The study investigates the influence of coordinating additives on lithium ion migration in ionic liquid mixtures, showing that strongly coordinating additives can reverse lithium migration direction and increase drift of neutral molecules. This effect depends strongy on the chelating ability of the additive, with strongly coordinating additives forming chelates with the Li ion to enhance its drift velocity.

JOURNAL OF PHYSICAL CHEMISTRY C (2021)

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Article Chemistry, Physical

NMR Parameters of Imidazolium Ionic Liquids as Indicators of Their State and Properties in Aqueous Solutions

A. A. Shahkhatuni et al.

Summary: The study found that the NMR chemical shifts and spin-spin coupling constants of ILs are significantly influenced by different anions, alkyl chain lengths, and water content. The addition of water can significantly alter some NMR parameters, while others remain relatively unchanged, indicating that these parameters reflect contributions from different properties of ILs.

JOURNAL OF SOLUTION CHEMISTRY (2021)

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Article Chemistry, Multidisciplinary

Confusing Ions on Purpose: How Many Parent Acid Molecules Can Be Incorporated in a Herbicidal Ionic Liquid?

Julia L. Shamshina et al.

Summary: This study aimed to expand the application range of herbicidal ionic liquids by increasing the amount of the systemic herbicide dicamba in its HILs. The research explored the influence of different salts on composition, finding that the maximum amount of HDic that can be accommodated in these formulations is a 1:4 M ratio.

ACS SUSTAINABLE CHEMISTRY & ENGINEERING (2021)

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Article Chemistry, Multidisciplinary

An Investigation into Interactions between 1-Butyl-3-methyl-imidazolium Tetrafluoroborate Guest and Pillar[5]arene Hosts: An Experimental and Molecular Dynamics Approach

Hamad H. Al Mamari et al.

Summary: Synthesized pillar[5]arene macrocycles were allowed to form complexes with the ionic liquid, and the complexation was confirmed through various spectroscopic techniques and molecular dynamics simulations.

CHEMISTRYSELECT (2021)

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Article Chemistry, Physical

Olefin epoxidation with ionic liquid catalysts formed by supramolecular interactions

Bingjie Ding et al.

Summary: This study demonstrated the design of specific ionic liquids through supramolecular complexation between 18-crown-6 and ammonium peroxoniobate, showing high catalytic activity in the presence of hydrogen peroxide. Various characterization techniques were used to confirm the properties of these ILs and their potential applications in epoxidation reactions.

MOLECULAR CATALYSIS (2021)

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Article Chemistry, Physical

Effect of rotating magnetic field on the diffusivity of ethylammonium nitrate ionic liquid confined between micrometer-spaced glass plates

Andrei Filippov et al.

Summary: The diffusion coefficient in layers of EAN confined between glass plates placed in a strong magnetic field is affected by the rotational conditions and duration of exposure to the magnetic field. While rotation along the magnetic field axis leads to a decrease in diffusion coefficient over time, rotation perpendicular to the magnetic field axis shows no effect on the diffusion coefficient until the rotation stops. Extended exposure to a static magnetic field can cause an increase in diffusivity when the sample starts to rotate around the axis perpendicular to the magnetic field.

JOURNAL OF MOLECULAR LIQUIDS (2021)

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Article Chemistry, Physical

Characterization of the ionic liquid obtained by chlorosulfonation of 1-methylimidazole: 1-methyl-3-sulfonic acid imidazolium chloride, 1-methylimidazolium chlorosulfate or a zwitterionic salt?

Bela Urban et al.

Summary: Numerous organic reactions catalyzed by the ionic liquid product of chlorosulfonation of 1-methylimidazole have been reported recently. Controversial assumptions on the real structure of the catalyst have emerged, but it has now been confirmed to be 1-methylimidazolium chlorosulfate. This structure was verified through X-ray crystallography and NMR spectroscopy, with experiments supporting rapid hydrolysis in the presence of water traces.

JOURNAL OF MOLECULAR LIQUIDS (2021)

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Article Chemistry, Physical

The unseen evidence of Reduced Ionicity: The elephant in (the) room temperature ionic liquids

Alessandro Mariani et al.

Summary: This study investigates the quantification of proton transfer in Protic Ionic Liquids (PILs) and introduces the concept of reduced ionicity to differentiate it from ionicity, shedding light on the relationship between acid strength, anion coordination power, and the properties of PILs. By combining various techniques and transport properties analysis, the research provides insights into the proton transfer and the modified behavior caused by reduced ionicity.

JOURNAL OF MOLECULAR LIQUIDS (2021)

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Article Chemistry, Physical

Anion-cation interactions in novel ionic liquids based on an asymmetric sulfonimide anion observed by NMR and MD simulations

Derick Gyabeng et al.

Summary: The interaction between ions in two novel ionic liquids containing DFTFSI anion was investigated, showing that the protonated end of DFTFSI preferentially interacts with IL cations. MD simulations also revealed hydrogen bonding interactions between DFTFSI and methoxy-functionalised cation, explaining the lower ionic conductivity and higher density in this IL compared to the C(3)mpyr DFTFSI system.

JOURNAL OF MOLECULAR LIQUIDS (2021)

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Article Chemistry, Physical

Cetylpyridinium picrate: Spectroscopy, conductivity and DFT investigation of the structure of a new ionic liquid

Maksym Fizer et al.

Summary: A new cetylpyridinium picrate ionic liquid was synthesized and characterized using various spectroscopic techniques, revealing properties such as phase transition from solid to liquid, interionic charge-transfer interactions, and molecular structures.

JOURNAL OF MOLECULAR STRUCTURE (2021)

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Article Chemistry, Physical

Rapid relaxation NMR measurements to predict rate coefficients in ionic liquid mixtures. An examination of reaction outcome changes in a homologous series of ionic liquids

Daniel C. Morris et al.

Summary: The study examined a series of ionic liquids based on 1-alkyl-3-methylimidazolium cations as components of a solvent mixture for a bimolecular substitution process. It found that changing the alkyl chain length or the amount of ionic liquid affected the rate coefficient of the process and NMR spin-spin relaxation of the solvent components. The study also determined that the activation parameters showed a step change when increasing the alkyl chain length, suggesting notable structuring in solution.

PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2021)

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Article Chemistry, Physical

Quantification of cation-cation, anion-anion and cation-anion correlations in Li salt/glyme mixtures by combining very-low-frequency impedance spectroscopy with diffusion and electrophoretic NMR

Sandra Pfeifer et al.

Summary: The study quantifies correlations between different ions in concentrated battery electrolytes, finding that all correlations are negative, with like-ion anticorrelations being particularly strong.

PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2021)

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Article Chemistry, Physical

Insights into the translational and rotational dynamics of cations and anions in protic ionic liquids by means of NMR fast-field-cycling relaxometry

Viviane Overbeck et al.

Summary: This study investigates the translational and rotational dynamics of cations and anions in triethylammonium based PILs using NMR Fast-Field-Cycling relaxometry. Diffusion coefficients and rotational correlation times of both ions were determined, with cations showing higher diffusion coefficients compared to anions. The results were compared with other methods and discussions were made on the relationship between ionic mobility and bulk viscosity.

PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2021)

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Article Chemistry, Multidisciplinary

Impact of Cellulose Dissolution on 1-Butyl-3-Methylimidazolium Chloride Crystallization Studied by Raman Spectroscopy, Wide-Angle X-ray Scattering, and Solid-State NMR

Nikolay Kotov et al.

CRYSTAL GROWTH & DESIGN (2020)

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Solvate Cation Migration and Ion Correlations in Solvate Ionic Liquids

Florian Schmidt et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2020)

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Understanding the Nature of Nuclear Magnetic Resonance Relaxation by Means of Fast-Field-Cycling Relaxometry and Molecular Dynamics Simulations-The Validity of Relaxation Models

Philipp Honegger et al.

JOURNAL OF PHYSICAL CHEMISTRY LETTERS (2020)

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Article Chemistry, Multidisciplinary

Spectral deconvolution in electrophoretic NMR to investigate the migration of neutral molecules in electrolytes

Florian Schmidt et al.

MAGNETIC RESONANCE IN CHEMISTRY (2020)

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Article Chemistry, Physical

Interactions and Transport in Highly Concentrated LiTFSI-based Electrolytes

Viktor Nilsson et al.

CHEMPHYSCHEM (2020)

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Structure Effects on the Ionicity of Protic Ionic Liquids

Sarah K. Mann et al.

CHEMPHYSCHEM (2020)

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Understanding the Interaction of Boric Acid and CO2 with Ionic Liquids in Aqueous Medium by Multinuclear NMR Spectroscopy

Andrei Filippov et al.

ACS SUSTAINABLE CHEMISTRY & ENGINEERING (2020)

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Sn-based Alloys Synthesized in an Ionic Liquid at Room Temperature: Cu6Sn5 as a Case Study

Nadia Soulmi et al.

CHEMNANOMAT (2020)

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Anions as Dynamic Probes for Ionic Liquid Mixtures

Maria Enrica Di Pietro et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2020)

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MAS NMR Investigation of Molecular Order in an Ionic Liquid Crystal

Sarah K. Mann et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2020)

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Tungstate ionic liquids as catalysts for CO2 fixation into epoxides

Roberto Calmanti et al.

MOLECULAR CATALYSIS (2020)

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Effects of ionicity and chain structure on the physicochemical properties of protic ionic liquids

Yuyan Deng et al.

AICHE JOURNAL (2020)

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NMR Spectroscopic Studies of Cation Dynamics in Symmetrically-Substituted Imidazolium-Based Ionic Liquid Crystals

Debashis Majhi et al.

INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES (2020)

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Xenon Dynamics in Ionic Liquids: A Combined NMR and MD Simulation Study

Franca Castiglione et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2020)

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NMR Relaxometry and Diffusometry Analysis of Dynamics in Ionic Liquids and lonogels for Use in Lithium-Ion Batteries

Nishani Kanchana Jayakody et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2020)

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Freezing the Motion in Hydroxy-Functionalized Ionic Liquids- Temperature Dependent NMR Deuteron Quadrupole Coupling Constants for Two Types of Hydrogen Bonds Far below the Glass Transition

Alexander E. Khudozhitkov et al.

JOURNAL OF PHYSICAL CHEMISTRY LETTERS (2020)

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Chloroaluminate Liquid Clathrates: Is It the Cations or the Anions That Drive the Solubility of Aromatics?

Rajkumar Kore et al.

INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH (2020)

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On the molecular mechanisms of α and β relaxations in ionic liquids

Elisa Steinruecken et al.

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Cation-Anion and Anion-CO2 Interactions in Triethyl(octyl)phosphonium Ionic Liquids with Aprotic Heterocyclic Anions (AHAs)

Seungmin Oh et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2020)

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Structural and Ion Dynamics in Fluorine-Free Oligoether Carboxylate Ionic Liquid-Based Electrolytes

Faiz Ullah Shah et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2020)

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Dynamics of Ionic Liquids in Confinement by Means of NMR Relaxometry-EMIM-FSI in a Silica Matrix as an Example

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Probing relaxation models by means of Fast Field-Cycling relaxometry, NMR spectroscopy and molecular dynamics simulations: Detailed insight into the translational and rotational dynamics of a protic ionic liquid

Viviane Overbeck et al.

JOURNAL OF MOLECULAR LIQUIDS (2020)

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Deep compositional understanding of TBA: AlCl3 ionic liquid for its applications

Mangesh Sakhalkar et al.

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Multi-spectroscopic monitoring of molecular interactions between an amino acid-functionalized ionic liquid and potential anti-Alzheimer's drugs

Srishti Sharma et al.

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Computational NMR Study of Ion Pairing of 1-Decyl-3-methyl-imidazolium Chloride in Molecular Solvents

Dovile Lengvinaite et al.

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Clusters of Hydroxyl-Functionalized Cations Stabilized by Cooperative Hydrogen Bonds: The Role of Polarizability and Alkyl Chain Length

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Heterogeneous Structures of Ionic Liquids as Probed by CO Rotation with Nuclear Magnetic Resonance Relaxation Analysis and Molecular Dynamics Simulations

Takatsugu Endo et al.

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Ionicity of deep eutectic solvents by Walden plot and pulsed field gradient nuclear magnetic resonance (PFG-NMR)

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Amphiphilic ionic liquid induced fusion of phospholipid liposomes

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NMR investigations on binding and dynamics of imidazolium-based ionic liquids with HEWL

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2020)

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Proton-deuterium exchange of acetone catalyzed in imidazolium-based ionic liquid-D2O mixtures

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Counting cations involved in cationic clusters of hydroxy-functionalized ionic liquids by means of infrared and solid-state NMR spectroscopy

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CO2 absorption and ion mobility in aqueous choline-based ionic liquids

Andrei Filippov et al.

JOURNAL OF MOLECULAR LIQUIDS (2019)

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Proton Transfer and lonicity: An 15N NMR Study of Pyridine Base Protonation

Mohammad Hasani et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2019)

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Molecular Mobility in a Set of Imidazolium-Based Ionic Liquids [bmim]+A- by the NMR-Relaxation Method

Sergei S. Bystrov et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2019)

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Article Chemistry, Multidisciplinary

Nuclear magnetic relaxation and diffusion study of the ionic liquids 1-ethyl- and 1-butyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide confined in porous glass

Amin Ordikhani Seyedlar et al.

MAGNETIC RESONANCE IN CHEMISTRY (2019)

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Investigating Intermolecular Interactions in a DME-Based Hybrid Ionic Liquid Electrolyte by HOESY NMR

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FRONTIERS IN CHEMISTRY (2019)

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Synthesis, characterization and catalytic activity of ionic liquid mimic halides modified MCM-41 for solvent free synthesis of phenyl glycidyl carbonate

R. Jothi Ramalingam et al.

MATERIALS CHEMISTRY AND PHYSICS (2019)

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How green are ionic liquids? - A multicriteria decision analysis approach

Marta Bystrzanowska et al.

ECOTOXICOLOGY AND ENVIRONMENTAL SAFETY (2019)

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Reactivity of CO2 with aqueous choline-based ionic liquids probed by solid-state NMR spectroscopy

Andrei Filippov et al.

JOURNAL OF MOLECULAR LIQUIDS (2019)

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Protic ionic liquid plus water interactions studied by 1D NOESY NMR spectroscopy

Dheiver Santos et al.

JOURNAL OF MOLECULAR STRUCTURE (2019)

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Possible Proton Conduction Mechanism in Pseudo-Protic Ionic Liquids: A Concept of Specific Proton Conduction

Hikari Watanabe et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2019)

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Charge Transport in Nonstoichiometric 2-Fluoropyridinium Triflate Protic Ionic Liquids

Patric Jannasch et al.

JOURNAL OF PHYSICAL CHEMISTRY C (2019)

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Effect of the Alkyl Chain Length of Amphiphilic Ionic Liquids on the Structure and Dynamics of Model Lipid Membranes

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LANGMUIR (2019)

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Effect of mixed anions on the transport properties and performance of an ionic liquid-based electrolyte for lithium-ion batteries

Victor Chaudoy et al.

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Hydrogen Bonding Between Ions of Like Charge in Ionic Liquids Characterized by NMR Deuteron Quadrupole Coupling Constants-Comparison with Salt Bridges and Molecular Systems

Alexander E. Khudozhitkov et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2019)

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On the relation between reorientation and diffusion in glass-forming ionic liquids with micro-heterogeneous structures

Manuel Becher et al.

JOURNAL OF CHEMICAL PHYSICS (2019)

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Translational Diffusion in a Set of Imidazoliunn-Based Ionic Liquids [bmim]+A- and Their Mixtures with Water

Sergei S. Bystrov et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2019)

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Dynamics of ionic liquids in poly(vinyl alcohol) porous scaffold. Low field NMR study

Carlos Mattea et al.

MAGNETIC RESONANCE IMAGING (2019)

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Comparison of fast field-cycling magnetic resonance imaging methods and future perspectives

Markus Boedenler et al.

MOLECULAR PHYSICS (2019)

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Molecular and Segmental Orientational Order in a Smectic Mesophase of a Thermotropic Ionic Liquid Crystal

Jing Dai et al.

CRYSTALS (2019)

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Controlled grafting of dialkylphosphonate-based ionic liquids on γ-alumina: design of hybrid materials with high potential for CO2 separation applications

M. A. Pizzoccaro-Zilamy et al.

RSC ADVANCES (2019)

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Article Chemistry, Physical

Molecular dynamics involving proton exchange of a protic ionic liquid-water mixture studied by NMR spectroscopy

Mohammad Hasani et al.

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Dynamics of [Pyr13][Tf2N] ionic liquid confined to carbon black

Steffen Merz et al.

PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2019)

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Article Chemistry, Physical

Simultaneous determination of deuteron quadrupole coupling constants and rotational correlation times: the model case of hydrogen bonded ionic liquids

A. E. Khudozhitkov et al.

PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2019)

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Article Chemistry, Multidisciplinary

Reorientation dynamics and ion diffusivity of neat dimethylimidazolium dimethylphosphate probed by NMR spectroscopy

Christoph Wiedemann et al.

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Article Chemistry, Physical

Dealing with supramolecular structure for ionic liquids: a DOSY NMR approach

Marcileia Zanatta et al.

PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2019)

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Formation of ionic liquid submicron particles. 1H and 19F nuclear magnetic resonance spectroscopic studies

Shigehiko Takegami et al.

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Article Chemistry, Multidisciplinary

Determining the relative strengths of aromatic and aliphatic C-H•••X hydrogen bonds in imidazolium ionic liquids through measurement of H/D isotope effects on 19F nuclear shielding

Gualberto Bottini et al.

MAGNETIC RESONANCE IN CHEMISTRY (2018)

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Article Chemistry, Multidisciplinary

Determination of inter-ionic and intra-ionic interactions in a monofluorinated imidazolium ionic liquid by a combination of X-ray crystallography and NOE NMR spectroscopy

Yves Lingscheid et al.

MAGNETIC RESONANCE IN CHEMISTRY (2018)

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Ion pair and solvation dynamics of [Bmim][BF4] + water system

Joao Cascao et al.

MAGNETIC RESONANCE IN CHEMISTRY (2018)

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Molecular mobility in several imidazolium-based ionic liquids according to data of H-1 and C-13 NMR relaxation

Vladimir V. Matveev et al.

MAGNETIC RESONANCE IN CHEMISTRY (2018)

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Dynamics of binary mixtures of an ionic liquid and ethanol by NMR

Amin Ordikhani Seyedlar et al.

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Multinuclear NMR and diffusion studies of quaternary amine-based ionic liquids

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A review of NMR methods used in the study of the structure and dynamics of ionic liquids

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Microheterogeneity in imidazolium and piperidinium cation-based ionic liquids: 1D and 2D NMR studies

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Average Intermolecular Distances and Dynamics of Ruthenium-Containing Organometallic Ionic Liquids Studied by Nuclear Overhauser Effects between 19F and 1H Nuclei and NMR Relaxation Rate Measurements

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Relevance of ion clusters for Li transport at elevated salt concentrations in [Pyr(12O1)][FTFSI] ionic liquid-based electrolytes

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Dynamical heterogeneities in ionic liquids as revealed from deuteron NMR

Alexander E. Khudozhitkov et al.

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Rotational and translational dynamics and their relation to hydrogen bond lifetimes in an ionic liquid by means of NMR relaxation time experiments and molecular dynamics simulation

Anne Strate et al.

JOURNAL OF CHEMICAL PHYSICS (2018)

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NMR relaxometric probing of ionic liquid dynamics and diffusion under mesoscopic confinement within bacterial cellulose ionogels

Chip J. Smith et al.

JOURNAL OF CHEMICAL PHYSICS (2018)

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Amphiphilic Ionic Liquid-Induced Membrane Permeabilization: Binding Is Not Enough

Sandeep Kumar et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2018)

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Evidences for Inclusion and Encapsulation of an Ionic liquid with β-CD and 18-C-6 in Aqueous Environments by Physicochemical Investigation

Koyeli Das et al.

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Article Chemistry, Physical

Improved Li-Ion Transport by DME Chelation in a Novel Ionic Liquid-Based Hybrid Electrolyte for Li-S Battery Application

Urbi Pal et al.

JOURNAL OF PHYSICAL CHEMISTRY C (2018)

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Probing Ionic Liquid Electrolyte Structure via the Glassy State by Dynamic Nuclear Polarization NMR Spectroscopy

Marc-Antoine Sani et al.

JOURNAL OF PHYSICAL CHEMISTRY LETTERS (2018)

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Article Optics

Hydrogen bonding in protic ionic liquids: structural correlations, vibrational spectroscopy, and rotational dynamics of liquid ethylammonium nitrate

Tobias Zentel et al.

JOURNAL OF PHYSICS B-ATOMIC MOLECULAR AND OPTICAL PHYSICS (2018)

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Molecular transport in ionic liquids under confinement studied by low field NMR

Carlos Mattea et al.

MICROPOROUS AND MESOPOROUS MATERIALS (2018)

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Selective binding and dynamics of imidazole alkyl sulfate ionic liquids with human serum albumin and collagen - a detailed NMR investigation

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2018)

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Intermolecular hydrogen bonds in water@IL supramolecular complexes

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On the measurement of intermolecular heteronuclear cross relaxation rates in ionic liquids

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Magnetic field effects dynamics of ethylammonium nitrate ionic liquid confined between glass plates

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2018)

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Negative effective Li transference numbers in Li salt/ionic liquid mixtures: does Li drift in the Wrong'' direction?

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2018)

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The influence of like-charge attraction on the structure and dynamics of ionic liquids: NMR chemical shifts, quadrupole coupling constants, rotational correlation times and failure of Stokes-Einstein-Debye

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2018)

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Multiscale nuclear magnetic relaxation dispersion of complex liquids in bulk and confinement

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PROGRESS IN NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY (2018)

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Selective observation of charge storing ions in supercapacitor electrode materials

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SOLID STATE NUCLEAR MAGNETIC RESONANCE (2018)

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Aqueous acidic solution - ionic liquid biphasic system: An original investigation by diffusion ordered spectroscopy nuclear magnetic resonance

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JOURNAL OF MOLECULAR LIQUIDS (2018)

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Investigation of Li+ Cation Coordination and Transportation, by Molecular Modeling and NMR Studies, in a LiNTf2-Doped Ionic Liquid-Vinylene Carbonate Mixture

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Microscopic and Macroscopic Properties of Carbohydrate Solutions in the Ionic Liquid 1-Ethyl-3-methyl-imidazolium Acetate

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JOURNAL OF PHYSICAL CHEMISTRY B (2018)

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Interfacial Behavior of Orthoborate Ionic Liquids at Inorganic Oxide Surfaces Probed by NMR, IR, and Raman Spectroscopy

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JOURNAL OF PHYSICAL CHEMISTRY C (2018)

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Transport properties and intermolecular interactions in binary mixtures based on the protic ionic liquid ethylimidazolium triflate and ethylene glycol

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2018)

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Intermolecular interactions upon carbon dioxide capture in deep-eutectic solvents

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Prediction of H-1 NMR chemical shifts for ionic liquids: strategy and application of a relative reference standard

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RSC ADVANCES (2018)

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Correlating Intermolecular Cross-Relaxation Rates with Distances and Coordination Numbers in Ionic Liquids

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JOURNAL OF PHYSICAL CHEMISTRY LETTERS (2018)

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Nonstoichiometric Triazolium Protic Ionic Liquids for All-Organic Batteries

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ACS APPLIED ENERGY MATERIALS (2018)

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1H NMR at Larmor frequencies down to 3 Hz by means of Field-Cycling techniques

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JOURNAL OF MAGNETIC RESONANCE (2017)

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Rotational dynamics of carbon dioxide in ionic liquids

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JOURNAL OF MOLECULAR LIQUIDS (2017)

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Understanding the Microscopic Behavior of the Mixture of Ionic Liquid/Ethylene Glycol/Lithium Salt through Time-Resolved Fluorescence, Nuclear Magnetic Resonance (NMR), and Electron Paramagnetic Resonance (EPR) Studies

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1H NMR Relaxometry and Diffusometry Study of Magnetic and Nonmagnetic Ionic Liquid-Based Solutions: Cosolvent and Temperature Effects

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JOURNAL OF PHYSICAL CHEMISTRY B (2017)

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Cation Dynamics in Supercooled and Solid Alkyl Methylimidazolium Bromide Ionic Liquids

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JOURNAL OF PHYSICAL CHEMISTRY B (2017)

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Solute Rotation in Ionic Liquids: Size, Shape, and Electrostatic Effects

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Ionicity of Protic Ionic Liquid: Quantitative Measurement by Spectroscopic Methods

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Investigation of Dynamics in BMIM TFSA Ionic Liquid through Variable Temperature and Pressure NMR Relaxometry and Diffusometry

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JOURNAL OF THE ELECTROCHEMICAL SOCIETY (2017)

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Transport properties and ionicity of phosphonium ionic liquids

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2017)

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Controlling the kinetic and thermodynamic stability of cationic clusters by the addition of molecules or counterions

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Quantitative assessment of kosmotropicity of hydrated ionic liquids by nuclear magnetic resonance

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Effect of mixed anions on the physicochemical properties of a sodium containing alkoxyammonium ionic liquid electrolyte

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2017)

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Achieving enhanced ionic mobility in nanoporous silica by controlled surface interactions

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Correlated/non-correlated ion dynamics of charge-neutral ion couples: the origin of ionicity in ionic liquids

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2017)

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Ion dynamics in halogen-free phosphonium bis(salicylato)borate ionic liquid electrolytes for lithium-ion batteries

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2017)

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Molecular dynamics of 1-ethyl-3-methylimidazolium triflate ionic liquid studied by 1H and 19F nuclear magnetic resonances

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2017)

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Alternative probe for the determination of the hydrogen-bond acidity of ionic liquids and their aqueous solutions

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Dynamical properties of EMIM-SCN confined in a SiO2 matrix by means of 1H NMR relaxometry

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PHYSICAL CHEMISTRY CHEMICAL PHYSICS (2017)

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Prediction of 1H NMR chemical shifts for clusters of imidazolium-based ionic liquids

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Phosphonium-phosphates/thiophosphates: Ionic liquids or liquid ion pairs? NMR spectroscopic classification

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TETRAHEDRON LETTERS (2017)

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NMR and Rheological Study of Anion Size Influence on the Properties of Two Imidazoliumbased Ionic Liquids

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Transport and Association of Ions in Lithium Battery Electrolytes Based on Glycol Ether Mixed with Halogen-Free Orthoborate Ionic Liquid

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SCIENTIFIC REPORTS (2017)

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Structure and dynamics elucidation of ionic liquids using multidimensional Laplace NMR

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Characterization of Doubly Ionic Hydrogen Bonds in Protic Ionic Liquids by NMR Deuteron Quadrupole Coupling Constants: Differences to H-bonds in Amides, Peptides, and Proteins

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CP MAS Kinetics Study of Ionic Liquids Confined in Mesoporous Silica: Convergence of Non-Classical and Classical Spin Coupling Models

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CHEMICAL COMMUNICATIONS (2017)

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Competition between Cation-Solvent and Cation-Anion Interactions in Imidazolium Ionic Liquids with Polar Aprotic Solvents

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The Electrochemical Synthesis of Polycationic Clusters

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ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2016)

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Probing the Aggregation Behavior of Neat Imidazolium-Based Alkyl Sulfate (Alkyl = Ethyl, Butyl, Hexyl, and Octyl) Ionic Liquids through Time Resolved Florescence Anisotropy and NMR and Fluorescence Correlation Spectroscopy Study

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Slow Molecular Motions in Ionic Liquids Probed by Cross-Relaxation of Nuclear Spins During Overhauser Dynamic Nuclear Polarization

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ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2016)

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Sample Shuttling Relaxometry of Contrast Agents: NMRD Profiles above 1 T with a Single Device

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In Situ MRI of Operating Solid-State Lithium Metal Cells Based on Ionic Plastic Crystal Electrolytes

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Comparative Investigation of the Ionicity of Aprotic and Protic Ionic Liquids in Molecular Solvents by using Conductometry and NMR Spectroscopy

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CO2 Absorption Properties and Mechanisms for 1-Ethyl-3-methylimidazolium Ether-Functionalized Carboxylates

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INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH (2016)

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About the nanostructure of the ternary system water - [BMIm]PF6 - TX-100

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Structure and molecular dynamics of sodium dodecylsulfate micelles modified with hydrophilic short-chain imidazolium salts in aqueous solution

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Detrimental effect of glass sample tubes on investigations of BF4--based room temperature ionic liquid-water mixtures

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Effect of Structure on Transport Properties (Viscosity, Ionic Conductivity, and Self-Diffusion Coefficient) of Aprotic Heterocyclic Anion (AHA) Room Temperature Ionic Liquids. 2. Variation of Alkyl Chain Length in the Phosphonium Cation

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Micellization Behavior of Surface Active Ionic Liquids Having Aromatic Counterions in Aqueous Media

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NMR Characterization of Ionicity and Transport Properties for a Series of Diethylmethylamine Based Protic Ionic Liquids

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JOURNAL OF PHYSICAL CHEMISTRY B (2016)

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Rotational Dynamics in Ionic Liquids from NMR Relaxation Experiments and Simulations: Benzene and 1-Ethyl-3-Methylimidazolium

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JOURNAL OF PHYSICAL CHEMISTRY B (2016)

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Electrochemical and Transport Properties of Ions in Mixtures of Electroactive Ionic Liquid and Propylene Carbonate with a Lithium Salt for Lithium-Ion Batteries

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Self-diffusion of phosphonium Bis(Salicylato)Borate ionic liquid in pores of Vycor porous glass

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MICROPOROUS AND MESOPOROUS MATERIALS (2016)

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Deuteron quadrupole coupling constants and reorientational correlation times in protic ionic liquids

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Polyiodides in room-temperature ionic liquids

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Structural origin of proton mobility in a protic ionic liquid/imidazole mixture: insights from computational and experimental results

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Insights into the effect of CO2 absorption on the ionic mobility of ionic liquids

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Dynamics of ionic liquids in bulk and in confinement by means of 1H NMR relaxometry - BMIM-OcSO4 in an SiO2 matrix as an example

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Understanding the mechanism of CO2 capture by 1,3 di-substituted imidazolium acetate based ionic liquids

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Local coordination and dynamics of a protic ammonium based ionic liquid immobilized in nano-porous silica micro-particles probed by Raman and NMR spectroscopy

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Li+ ion transport in ionic liquid-based electrolytes and the influence of sulfonate-based zwitterion additives

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A remarkable chiral recognition of racemic Mosher's acid salt by naturally derived chiral ionic liquids using 19F NMR spectroscopy

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Exceptional activity of gallium(III) chloride and chlorogallate(III) ionic liquids for Baeyer-Villiger oxidation

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Design of Phosphonated Imidazolium-Based Ionic Liquids Grafted on γ-Alumina: Potential Model for Hybrid Membranes

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INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES (2016)

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Viscous Calibration Liquids for Self-Diffusion Measurements

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The intermolecular NOE is strongly influenced by dynamics

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IONICS (2015)

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High-resolution slice selection NMR for the measurement of CO2 diffusion under non-equilibrium conditions

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Ionization dynamics in ionic liquids probed via self-diffusion coefficient measurements

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Pair dynamics and the intermolecular nuclear Overhauser effect (NOE) in liquids analysed by simulation and model theories: Application to an ionic liquid

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19F spin-lattice relaxation of perfluoropolyethers: Dependence on temperature and magnetic field strength (7.0-14.1 T)

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Molecular interactions in the ionic liquid emim acetate and water binary mixtures probed via NMR spin relaxation and exchange spectroscopy

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Probing the effect of electron donation on CO2 absorbing 1,2,3-triazolide ionic liquids

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RSC ADVANCES (2014)

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From Short-Range to Long-Range Intermolecular NOEs in Ionic Liquids: Frequency Does Matter

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ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2013)

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Interactions in 1-ethyl-3-methyl imidazolium tetracyanoborate ion pair: Spectroscopic and density functional study

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Understanding the effect of side groups in ionic liquids on carbon-capture properties: a combined experimental and theoretical effort

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Radiation damping in modern NMR experiments: Progress and challenges

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PROGRESS IN NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY (2013)

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Heteronuclear NOE Spectroscopy of Ionic Liquids

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Spectroscopic and computational analysis of the molecular interactions in the ionic liquid ion pair [BMP]+[TFSI]-

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Nuclear magnetic resonance relaxometry as a method of measuring translational diffusion coefficients in liquids

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PHYSICAL REVIEW E (2012)

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Quadrupole relaxation enhancement-application to molecular crystals

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Et tu, Grotthuss! and other unfinished stories

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