4.4 Article

Microstructural evolution for a single-crystal superalloy after high-temperature treatments with different holding times

Journal

MATERIALS SCIENCE AND TECHNOLOGY
Volume 38, Issue 12, Pages 836-841

Publisher

TAYLOR & FRANCIS LTD
DOI: 10.1080/02670836.2022.2065737

Keywords

Single-crystal superalloys; surface recrystallisation; discontinuous precipitation; EBSD

Funding

  1. National Natural Science Foundation of China [52071012]
  2. Academic and Technical Leaders of Major Disciplines in Jiangxi Province [20182BCB22020]
  3. Xi'an Advanced Manufacturing Technology Project [21XJZZ0048]

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The thermal heating and cooling behavior of a single-crystal superalloy containing 2wt-% Re was investigated in this study to understand the dissolution process of gamma ' and the surface recrystallization behavior of grit-blasted superalloy near its ultimate service temperature of 1100 degrees C. Aged samples were vertically polished to observe the progress of the discontinuous precipitation reaction front. Microstructure characteristics, including grain orientation, grain size, texture, and TCP phase precipitation, were studied to gain a detailed understanding of the surface crystallization behavior of the material.
In the present work, the thermal heating and cooling behaviour of a single-crystal superalloy containing 2wt-% Re was tested to investigate the gamma ' dissolution process, and the surface recrystallisation behaviour of the grit-blasted superalloy was investigated near its ultimate service temperature of 1100 degrees C by EBSD and TEM. Particularly, the aged samples were vertically polished to reveal the progress of the discontinuous precipitation reaction front. The microstructure characteristics, including grain orientation, grain size, texture and TCP phase precipitation, were revealed for a detailed understanding of the surface crystallisation behaviour of the material.

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