Journal
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
Volume 842, Issue -, Pages -Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.msea.2022.143102
Keywords
H13 steel; Spray-forming; Microstructure; Fracture mechanism; High-temperature strength
Categories
Funding
- Science and Tech-nology Department of Jiangsu Province [BE2017127]
- Open Research Fund from the State Key Laboratory of Rolling and Automation, Northeastern University [2020RALKFKT017]
- Opening Project of Jiangsu Key Laboratory of Advanced Struc-tural Materials and Application Technology [ASMA202002]
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This study focuses on the improved high-temperature strength and mechanical properties of hot work die steels using modified SF01 steel. The modified SF01 steel exhibits higher yield strength and lower elongation compared to conventional H13 steel over a wide temperature range. The microstructural characteristics are correlated with the yield strength, and the unsatisfactory toughness of SF01 steel is attributed to the presence of VC.
The rapid development in the advanced manufacturing industry asks for better service performance of hot work die steels, especially their high-temperature strength. In this work, a modified SF01 steel based on H13 steel was spray-formed with the carbon content increased to 0.5 wt %. The yield strength (YS) and elongation of SF01 steel at 25 degrees C are about 1824 MPa and 8.6%, respectively, with YS improving by 14.6% and elongation decreasing by 9% compared to conventional H13 steel (about 1591 MPa, 9.6%). It was also found that the YS of SF01 steel was at least 10% larger than H13 steel over the temperature range from 25 to 650 degrees C. The average grain size of tempered SF01 steel is smaller, the dislocation density is lower, and the volume fraction of precipitations is larger than conventional H13 steel (CH13). Furthermore, M3C and VC were observed in tempered SF01 steel, which were not found in CH13. The finer grain size is ascribed to the combined effect of spray forming and the pinning of grain boundaries by VC during 1040 degrees C austenitization process in quenching. A mathematical model was utilized to correlate microstructural characteristics with yield strength. Calculations revealed that the superior YS of SF01 is ascribed to a higher contribution of grain boundary strengthening and precipitation strengthening. The unsatisfied toughness of SF01 steel results from the presence of VC with an average size of 440 nm, which could promote cracks nucleation in the brittle temperature range when subjected to tension loading, and help micropores initiation during plastic deformation. The brittle-to-ductile transition temperature of SF01 is about 200 degrees C, and the deformation mechanism from room temperature to 650 degrees C is briefly discussed.
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