4.7 Article

Multiscale investigation on fatigue properties and damage of a 3D braided SiC/SiC plus PyC/SiC composites in the full stress range at 1300 °C

Journal

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
Volume 42, Issue 4, Pages 1208-1218

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.jeurceramsoc.2021.11.045

Keywords

SiC; SiC composites; High-temperature fatigue; Failure mechanism; Multiscale investigation; Interfacial debonding strength

Funding

  1. National Natural Science Foundation of China [51772009, 51911530201, 51802264]
  2. Natural Science Foundation of Shanxi Province [2020JQ-177]
  3. Academic Excellence Foundation of BUAA

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By conducting monotonic tensile and fatigue tests of SiC/SiC composites at 1300 degrees C, it was found that the fatigue behaviors can be divided into three zones. In all three zones, inelastic strains accumulation and stiffness reduction were observed due to matrix cracking, interface damage, and failure of fibers. The fatigue life is long in the run-out zone when the maximum stress is lower than the proportional limit stress (PLS). In the stress-insensitive zone, fracture depends on high-temperature and oxidation effects. Failure in the stress-sensitive zone is dominated by the fiber strength. The interface behaviors greatly affect the fatigue life above the PLS.
Monotonic tensile and fatigue tests of a SiC/SiC composites were conducted at 1300 degrees C in the full stress range. The macroscopic behaviors were studied based on the strain data. The mesoscopic morphology was observed by X-ray computed tomography, and the microanalysis was conducted using SEM, EDS and XRD. Besides, the interfacial debonding strength (IDS) were measured by nano-indenter. The results reveal that the fatigue behaviors can be divided into three zones. The inelastic strains accumulation and stiffness reduction can be observed in all three zones due to matrix cracking, interface damage, and failure of fibers. The fatigue life is long in the run-out zone because the maximum stress is lower than the proportional limit stress (PLS). In the stressinsensitive zone, the fracture depends on high-temperature and oxidation effects. The failure in the stresssensitive zone is dominated by the fiber strength. The interface behaviors greatly affect the fatigue life above the PLS.

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