Journal
JOURNAL OF ANALYTICAL AND APPLIED PYROLYSIS
Volume 118, Issue -, Pages 1-8Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.jaap.2015.12.013
Keywords
Microwave; Hydrothermal carbonization; Carbonized material; Prosopis africana shell
Funding
- Petroleum Technology Development Fund (PTDF), Nigeria
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This study compares the chemical and structural properties of the hydrochars prepared from microwave-assisted and conventional hydrothermal carbonizations of Prosopis africana shell, a waste plant material. The preparation involved heating the raw material in de-ionized water at 200 degrees C for 5-20 min, and 120-240 min in the microwave and conventional oven respectively. The prepared hydrochars were characterized using the scanning electron microscope, nitrogen sorption measurement, Fourier transform infrared spectroscopy, CHN analyzer, thermogravimetric analysis, and nuclear magnetic resonance. The results showed that the microwave-assisted hydrothermal carbonization process is fast in the carbonization of the Prosopis africana shell as shown by the level of conversion attained within the short time. This study presents new data on the comparison of the hydrochars from microwave-assisted and conventional hydrothermal carbonization processes of the same lignocellulosic material in terms of their properties. (C) 2015 Elsevier B.V. All rights reserved.
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