Journal
JOURNAL OF SUPERCRITICAL FLUIDS
Volume 182, Issue -, Pages -Publisher
ELSEVIER
DOI: 10.1016/j.supflu.2022.105527
Keywords
Isopropanol; High pressure extraction; Essential fatty acids; Bioactive compounds; Phytosterols
Categories
Funding
- Fundacao de Amparo a Pesquisa do estado de Sao Paulo, Brazil (FAPESP) [2016/13460-8]
- Conselho Nacional de Desenvolvimento Cientifico e Tecnologico, Brazil (CNPq) [306317/2016-8]
- Fondo Nacional de Desarrollo Cientifico y Tecnologico, Peru (FONDECYT) [0242-2015]
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The aim of this study was to evaluate the effects of static time, contact time, and temperature on oil extraction yield, free fatty acids, total phenolic content, and beta-sitosterol content. The results showed that static time and temperature influenced extraction yield and total phenolic content, while beta-sitosterol content and fatty acids were not significantly affected.
The aim of this study was to evaluate the effects of the static time (St, 2-10 min), contact time between the solvent (pressurized isopropanol - 10.35 MPa) and the matrix (pequi or sacha inchi almonds) in each cycle and temperature (T, 60-90 degrees C) in the intermittent purging process for oil extraction yield (X-0), free fatty acids (FFAs), total phenolic content (TPC) and beta-sitosterol content. Fatty acid (FA) profiles were determined. The St and the T of the process influenced X-0 and TPC, but beta-sitosterol content and FFAs were not significantly affected. The higher beta-sitosterol content (31.71-57.22 mg/100 g of oil) and TPC (64.23-589.46 mg GAE/kg of oil) was presented sacha inchi and pequi oils, respectively. The main FA in sacha inchi and pequi oils were linolenic (18:3n-3; 44.03-47.13%) , oleic (18:1n-9; 48.28-50.77%) acid, respectively. The extraction with pressurized iso-propanol in 27 min allowed high oil recovery (92.98% for pequi and 86.55% for sacha inchi).
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