4.5 Article

Synthesis of light weight recron fiber-reinforced sodium silicate based silica aerogel blankets at an ambient pressure for thermal protection

Journal

JOURNAL OF POROUS MATERIALS
Volume 29, Issue 4, Pages 957-969

Publisher

SPRINGER
DOI: 10.1007/s10934-022-01231-3

Keywords

Industrial grade sodium silicate; Monolithic and robust silica aerogel blanket; Recron fiber; Ambient pressure drying; Porosity; Thermal stability; And flexibility

Funding

  1. University of Mumbai
  2. Department of Physics and University of Jeddah, Deanship of Scientific Research (DSR) [UJ-02-020-ICGR]
  3. DST-SERB project [EEQ/2020/0002980]

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In this study, lightweight recron fibers were added to silica sol to fabricate lightweight recron-based silica aerogel blankets (RSAB) with excellent flexibility, hydrophobicity, thermal stability, mechanical robustness, high porosity, and large BET surface area. The RSAB showed high water-repelling properties, thermal insulation performance, and potential for energy-saving applications in electrical appliances.
In this work, for the sake of improving the performance of homogeneous and flexible silica aerogel blankets in practical applications, lightweight recron fibers were added in silica sol for the fabrication of silica aerogel blankets. The recron based silica aerogel blanket (RSAB) was synthesized by using a low-cost industrial grade sodium silicate precursor with the superficial sol-gel process via ambient pressure drying technique. The as-synthesized RSAB features excellent flexibility, hydrophobic, thermally stable, and mechanical robustness. The Si-C-H bond percentage is maintained at 6% after heat treatment at 270 degrees C, which results in the high water-repelling phenomenon at a contact angle of 120 degrees. The thermal stability of the aerogel blanket is also confirmed (246 degrees C) by differential scanning calorimetry. Moreover, the prepared aerogel acquires 87% porosity with homogeneous microstructure and BET surface area as 644 m(2)/g. The oxidation peak is detected at 280 degrees C of -CH3 groups. The latter endowed the RSAB exhibits superior thermal insulation property as well as excellent flexibility. These prepared RSAB aerogel composites may have great integrity for a wide diversity of energy-saving applications. Such RASB can have great potential in electrical appliances for energy conservation purposes due to its lightweight, thermally stable, mechanically robust, highly flexible, and economical manufacturing processes.

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