4.6 Article

An indentation method for determining the film thickness, Young's modulus, and hardness of bilayer materials

Journal

JOURNAL OF PHYSICS D-APPLIED PHYSICS
Volume 55, Issue 27, Pages -

Publisher

IOP Publishing Ltd
DOI: 10.1088/1361-6463/ac5da6

Keywords

film-substrate system; Young's modulus; hardness; film thickness; weight function; instrumented indentation technique

Funding

  1. National Natural Science Foundation of China [12072324, 11702253, U1804254]
  2. Natural Science Foundation of Henan Province for Excellent Young Scholars [212300410087]

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This article proposes a method to solve the inverse problem of characterizing mechanical properties of bilayer materials using finite element simulation. The method can determine the film thickness, Young's modulus, and hardness of film and substrate. It has practical prospects in the field of indentation testing technology.
Simultaneously determining the film thickness, Young's modulus, and hardness of film and substrate is a significant challenge due to the substrate effect. A method to solve the inverse problem of characterizing the mechanical properties of bilayer materials for instrumented indentation testing is proposed. This is done in combination with a weight function which could be obtained via finite element simulation. Using the proposed method, the film thickness and Young's modulus of film-substrate materials, and the hardness values of the film and substrate could be determined. The proposed method is applicable to Vickers, Berkovich, and 70.3 degrees conical indenters. Within the study range, numerical and theoretical results show that this method is both feasible and accurate in determining the above parameters, compared with existing experimental results. The method flow chart to determine the above parameters is also shown. This method separates the coupling effect between the film and the substrate in the bilayer material, giving it practical prospects in the field of indentation testing technology.

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