Towards creep property improvement of selective laser melted Ni-based superalloy IN738LC

Nickel-based superalloy IN738LC produced by selective laser melting (SLM) exhibits inferior hightemperature creep properties than its cast counterparts due to relatively smaller grain size, particularly for the plane normal to the building direction. This work studied effects of post heating strategy on the microstructure and especially the grain size to improve the high temperature creep resistance. The asbuilt microstructure exhibited a fine grain size and large quantities of M C carbides that could effectively hinder grain growth. It was found that unconventional two-step heat treatments could lead to substantial grain growth, and the effect is particularly prominent at a specific temperature. The ease of grain growth was explained after classifying the microstructural evolution (boundary carbide transformation) during each heating step and related to the reduced grain boundary pinning force from M C carbides. Creep tests validated the effect of the new heat treatment scheme on the SLM-processed IN738LC at 850 degrees C. An extended creep fracture life (1.5 to 4 times improvement) and lower secondary creep rates were achieved with samples subjected to the newly optimized two-step heat treatment. The complete creep curves are also firstly presented for SLM-IN738LC, confirming the effectiveness of grain growth and highlighting the importance of dedicated heat treatment for SLM superalloys. (c) 2022 Published by Elsevier Ltd on behalf of The editorial office of Journal of Materials Science & Technology.

Automated summary

This study investigates the effects of post heating strategy on the microstructure and grain size of a nickel-based superalloy produced by selective laser melting (SLM), aiming to improve its high temperature creep resistance. Unconventional two-step heat treatments are found to lead to substantial grain growth, particularly at a specific temperature. The newly optimized two-step heat treatment scheme extends the creep fracture life and reduces secondary creep rates for the SLM-processed superalloy.