4.7 Article

Graded microstructure and properties of TiCp/Ti6Al4V composites manufactured by laser melting deposition

Journal

CERAMICS INTERNATIONAL
Volume 48, Issue 5, Pages 6985-6997

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2021.11.256

Keywords

Composites; Laser melting deposition; Graded microstructure; Microhardness

Funding

  1. National Key R&D Program of China [2017YFE0123500]
  2. Fundamental Research Funds for the Central Universities
  3. Natural Science Foundation of Heilongjiang Province, China [LH2019E028]
  4. China Postdoctoral Science Foundation [2019M651259]
  5. Open Project of State Key Laboratory of Advanced Welding and Joining [AWJ-22M17]

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In this paper, TiCp/Ti6Al4V composites were fabricated using laser melting deposition (LMD) technology and the microstructure and microhardness of different deposited layers were analyzed. The results show that the composites have a graded microstructure and microhardness distribution. The microhardness increases gradually from the bottom layer to the top layer in the low power composite, while the high power composite shows a more significant increase in microhardness.
In this paper, 50 vol% TiCp/Ti6Al4V composites without pores, cracks or poor fusion were fabricated by laser melting deposition (LMD) technology using 500 W laser power (lower power, LP) and 1000 W laser power (higher power, HP). The microstructure of different deposited layers was analyzed and the corresponding microhardness was measured. The results show that the composites are composed of undissolved TiC, in-situ TiC (eutectic TiC and primary TiC), alpha Ti and beta Ti. It is interesting that the microstructure from the bottom layer to the top layer presents a graded distribution when all layers have the same composition. The eutectic TiC is mainly formed in lower layers while the primary TiC is mainly in upper layers. With increasing layer number, the size and number of the primary TiC grains increase and the primary TiC grows gradually from granules into dendrites, however, the number of the undissolved TiC particles decreases along the depositing direction. The simulation results show that the peak temperature of deposited layer increases while the cooling rate decreases with increasing layer number. Different thermal history affects the diffusion of carbon and the evolution of TiC, and then affects the microstructure distribution of the composites. This graded microstructure leads to the graded distribution of microhardness. The microhardness of the LP composite rises from 432.5 HV to 488.1 HV, while the HP composite rises from 435.5 HV to 604.3 HV from the bottom layer to the top layer, respectively.

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