Dynamic precipitation and recrystallization mechanism during hot compression of Mg-Gd-Y-Zr alloy

Hot compression tests of Mg-Gd-Y-Zr alloy at different deformation temperatures and strains were carried out with Gleeble-1500 simulator at strain rate of 0.002 s-1. The microstructure evolution of 400 degrees C/0.002 s-1 sample under different strain was analyzed emphatically by transmission electron microscopy and electron backscatter diffraction technology. Dynamic precipitation characteristics and nucleation-expansion mechanism of dynamic recrystallization (DRX) were discussed in detail. The results indicated that the dynamic precipitation takes place prior to DRX, and the morphology, size and distribution of precipitates change with increasing strain. At the later stage of deformation, the large-size hard phase b-Mg5(Gd,Y) can induce the particle-stimulated nucleation (PSN) mechanism under large strain and act as an effective nucleation site for DRX. In addition, we constructed a schematic diagram of the DRX nucleation-expansion mechanism of Mg-Gd-Y-Zr alloy under high temperature deformation. The first layer of DRX grains is formed by discontinuous dynamic recrystallization (DDRX) mechanism characterized by grain boundary bulge out, and the precipitates distributed at the original grain boundary promote DDRX nucleation; The expansion of necklace structure depends on continuous dynamic recrystallization (CDRX) mechanism; Subgrain division can further refine DRX grains. (c) 2021 The Author(s). Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

Automated summary

In this study, the microstructure evolution and dynamic recrystallization mechanism of Mg-Gd-Y-Zr alloy under different deformation conditions were analyzed in detail. It was found that dynamic precipitation occurs prior to dynamic recrystallization, and large-size hard phase particles can induce dynamic recrystallization under high strain conditions, promoting grain refinement.