Polymer assisted colloidal nanocrystal framework synthesis: sol-gel approach

The porous colloidal nanocrystal framework material was synthesized by sol-gel assembly followed by a self-propagation procedure. The characteristics of the synthesized nanocrystal were confirmed by advanced instruments. From the DTG analysis, the poly (vinyl alcohol) was completely degraded at 400 degrees C. The XRD pattern and TEM image confirmed the nanoscale crystallite size of the material. BET and SEM analysis showed the mesoporous type pore size distribution. The predictable compositional analysis was confirmed from EDX, SAED, and XPS compositional analysis. Using the HSAB theory and HRTEM image analysis the formation of local heterojunction between metal oxides was approved.

Automated summary

The characteristics and structure of the synthesized porous colloidal nanocrystal framework material were confirmed using advanced instruments and analytical methods. The material showed complete degradation at high temperature, with nanoscale crystallite size and mesoporous structure. The composition and structure were predicted and confirmed through different compositional analysis methods.