4.2 Article

Single-shot experiments at the soft X-FEL FERMI using a back-side-illuminated scientific CMOS detector

Journal

JOURNAL OF SYNCHROTRON RADIATION
Volume 29, Issue -, Pages 103-110

Publisher

INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S1600577521012303

Keywords

CMOS; soft X-ray FEL applications; single-shot experiment; time resolved

Funding

  1. Agence Nationale de la Recherche [ANR-20-CE42-0012-01, ANR-15GRFL-0005, PCI2019-111908-2]
  2. Agence Nationale de la Recherche (ANR) [ANR-20-CE42-0012] Funding Source: Agence Nationale de la Recherche (ANR)

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The latest CMOS 2D sensors now rival photon detectors in performance for optical applications, combining high frame rate speeds with a wide dynamic range. A new generation of large back-side-illuminated scientific CMOS sensors has been developed, offering high efficiency and competitive performance. These sensors have been implemented and characterized, and their feasibility for single-shot ultra-fast experiments at FEL sources in the EUV/soft X-ray regime has been explored.
The latest Complementary Metal Oxide Semiconductor (CMOS) 2D sensors now rival the performance of state-of-the-art photon detectors for optical application, combining a high-frame-rate speed with a wide dynamic range. While the advent of high-repetition-rate hard X-ray free-electron lasers (FELs) has boosted the development of complex large-area fast CCD detectors in the extreme ultraviolet (EUV) and soft X-ray domains, scientists lacked such high-performance 2D detectors, principally due to the very poor efficiency limited by the sensor processing. Recently, a new generation of large back-side-illuminated scientific CMOS sensors (CMOS-BSI) has been developed and commercialized. One of these cost-efficient and competitive sensors, the GSENSE400BSI, has been implemented and characterized, and the proof of concept has been carried out at a synchrotron or laser-based X-ray source. In this article, we explore the feasibility of single-shot ultra-fast experiments at FEL sources operating in the EUV/soft X-ray regime with an AXIS-SXR camera equipped with the GSENSE400BSI-TVISB sensor. We illustrate the detector capabilities by performing a soft X-ray magnetic scattering experiment at the DiProi end-station of the FERMI FEL. These measurements show the possibility of integrating this camera for collecting single-shot images at the 50 Hz operation mode of FERMI with a cropped image size of 700 x 700 pixels. The efficiency of the sensor at a working photon energy of 58 eV and the linearity over the large FEL intensity have been verified. Moreover, on-the-fly time-resolved single-shot X-ray resonant magnetic scattering imaging from prototype Co/Pt multilayer films has been carried out with a time collection gain of 30 compared to the classical start-and-stop acquisition method performed with the conventional CCD-BSI detector available at the end-station.

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