Journal
APPLIED SCIENCES-BASEL
Volume 12, Issue 3, Pages -Publisher
MDPI
DOI: 10.3390/app12031215
Keywords
neutron reflectometry; liquid-liquid interface; air-liquid interface; adsorption structure; sodium dodecyl sulfate
Categories
Funding
- Japan Society of the Promotion of Science (JSPS) [(B) 17H03438, (B) 20H02497, (C) 21K05121]
- [2018I1605]
- [2020I1614]
- [2020B0005]
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Knowledge of interfacial structures in liquid-liquid systems is crucial for enhancing two-phase biological and chemical reactions. A new sample cell for neutron reflectometry (NR) was developed to observe the layer structure around the interface. The adsorption behavior of SDS on the toluene-D2O interface was investigated under the new experimental conditions.
Knowledge of interfacial structures in liquid-liquid systems is imperative, especially for improving two-phase biological and chemical reactions. Therefore, we developed a new sample cell for neutron reflectometry (NR), which enables us to observe the layer structure around the interface, and investigated the adsorption behavior of a typical surfactant, sodium dodecyl sulfate (SDS), on the toluene-d(8)-D2O interface under the new experimental conditions. The new cell was characterized by placing the PTFE frame at the bottom to produce a smooth interface and downsized compared to the conventional cell. The obtained NR profiles were readily analyzable and we determined a slight difference in the SDS adsorption layer structure at the interface between the toluene-d(8)-D2O and air-D2O systems. This could be owing to the difference in the adsorption behavior of the SDS molecules depending on the interfacial conditions.
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