Fabrication of Fe-Si-B Based Amorphous Powder Cores by Spark Plasma Sintered and Their Magnetic Properties

Mechanical ball milling was used to coat SiO2 nanopowder on a Fe-Si-B amorphous powder in this study. The Fe-Si-B/SiO2 core-shell amorphous composite powder was obtained after 6h of ball milling. At 490 degrees C, the amorphous powder is thermally stable. Discharge plasma sintering was used to create a Fe-Si-B/SiO2 magnetic powder core (SPS). At a sintering temperature of 420 to 540 degrees C, the phase composition and magnetic characteristics of the magnetic particle core were investigated. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) were used to examine the structural features of the magnetic particle core. A precision resistance tester and a vibrating sample magnetometer were used to assess the resistivity and magnetic characteristics of the magnetic particle core. The findings showed that Fe3Si and Fe2B are the phases generated during spark plasma sintering. High-frequency power loss increases as density rises. However, at the measured frequency, the magnetic permeability of the magnetic particle core changes slightly and has excellent frequency characteristics, making it appropriate for use in high-frequency components.

Automated summary

In this study, mechanical ball milling was used to coat SiO2 nanopowder on a Fe-Si-B amorphous powder, resulting in the formation of Fe-Si-B/SiO2 core-shell amorphous composite powder. Discharge plasma sintering was then employed to create a magnetic powder core, and the phase composition and magnetic characteristics of the core were investigated.