Journal
SYNTHETIC COMMUNICATIONS
Volume 52, Issue 3, Pages 402-412Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/00397911.2022.2028843
Keywords
Alkenoic acids; bromolactonization; electrochemical reaction; gamma-lactones
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Funding
- Soonchunhyang University
- Basic Science Research Program through the National Research Foundation of Korea [NRF-2021R1I1A3044807, 2021R1A6A1A03039503]
- National Research Foundation of Korea [2021R1A6A1A03039503] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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This study presents the development of an electrochemical method for bromination and cyclization reactions, which offers an environmentally friendly approach and enables efficient synthesis of bromomethylated gamma-lactone derivatives.
Electrochemical radical bromination and cyclization sequences of alkenoic acids developed in this study. This approach is environmental-friendly by using carbon tetrabromide as a bromine radical precursor. The electrochemical protocol offers a facile way to prepare bromomethylated gamma-lactones derivatives in moderate to high yields. [GRAPHICS] .
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