4.7 Review

Recent developments and trends in miniaturized gas preconcentrators for portable gas chromatography systems: A review

Journal

SENSORS AND ACTUATORS B-CHEMICAL
Volume 346, Issue -, Pages -

Publisher

ELSEVIER SCIENCE SA
DOI: 10.1016/j.snb.2021.130449

Keywords

Preconcentration; Miniaturization; Microfabrication; Gas chromatography; VOC detection; Normalized Preconcentration Efficacy (NPE)

Funding

  1. European Union [643095]
  2. Clean Sky 2 Joint Undertaking under the European Union's Horizon 2020 research and innovation program [687014]
  3. LIFE program [LIFE17 ENV/FR/000330]
  4. European project ELCOD
  5. European Regional Development Fund (ERDF)
  6. Region Grand Est in France
  7. H2020 Societal Challenges Programme [687014] Funding Source: H2020 Societal Challenges Programme

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Portable gas chromatography systems with integrated preconcentrators are crucial for achieving enhanced sensitivity in various analytical applications. This review focuses on recent advancements in preconcentrators, discussing materials, fabrication techniques, designs, heating technologies, adsorbents, and applications, as well as proposing a new performance metric, Normalized Preconcentration Efficacy (NPE), for standardized evaluation and comparison of devices.
In the last years, a growing number of fields such as air quality monitoring, breath analysis or explosives and chemical warfare agents detection requiring fast, on-site, sensitive analysis has led to the development of portable gas chromatography systems. In most cases, these systems integrate a miniaturized gas preconcentrator, which provides a significant enhancement of the sensitivity enabling quantification of analytes present in the sample at trace levels. In this review, the authors have focused on recent developments in these preconcentrators integrated in portable gas chromatography systems. The main materials and fabrication techniques, designs, heating technologies, fluidic connections, adsorbents, and applications are discussed. In addition, an analysis of some factors affecting preconcentration performance is presented. A new figure of merit called Normalized Preconcentration Efficacy (NPE) is proposed to evaluate the performance of these devices in a standardized manner, making possible a more straightforward comparison between different devices.

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