4.7 Article

Lifetime health monitoring of fiber reinforced composites using highly flexible and sensitive MXene/CNT film sensor

Journal

SENSORS AND ACTUATORS A-PHYSICAL
Volume 332, Issue -, Pages -

Publisher

ELSEVIER SCIENCE SA
DOI: 10.1016/j.sna.2021.113148

Keywords

MXene; CNT film sensor; Cure monitoring; Gel point; Structural health monitoring; Mechanical Properties

Funding

  1. National Natural Science Foundation of China [11902204]
  2. Liaoning Revitalization Talents Program [XLYC2007118]
  3. Aeronautical Science Foundation [201903054001]
  4. Natural Science Foundation of Liaoning Province [2020-MS-236, 2019010256-JH3/301]
  5. Shenyang Youth Technological Innovation Talent Project [RC200030, RC190004]

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This paper investigates the lifetime health monitoring of composites through the development of a highly sensitive MXene/CNT film sensor. The sensor shows good real-time performance and long service life, making it suitable for optimizing curing systems and improving the quality of composite products.
In this paper, lifetime health monitoring of composites was conducted, included manufactured monitoring and structural health monitoring. A thin film sensor composed of multi-walled carbon nanotubes (MWCNTs) and MXene was developed through simple mixing and spray vacuum filtration. This highly flexible and susceptible MXene/CNT film sensor can be embedded in polymer composites to monitor the phase change of the resin and the determination of the gel point during the preparation of the composite in real-time. The MXene/CNT film sensors were embedded and arrayed in fiber-reinforced composites, which can be used for resin curing monitoring, then continued structural health monitoring. Experimental results show that the MXene/CNT film sensor embedded in the composite laminates can effectively capture the change of the resin phase, that characterized by resistance. MXene/CNT films have a good ability to respond to changes in the resin state. The gel point of resin obtained from the MXene/CNT film sensor is 134 degrees C, which is consistent with 137 degrees C from the DMA results. The accurate gel point can optimize the curing system and improve the quality of composite products. Then the tensile, bending, and fatigue tests of fiber reinforced composite laminates embedded with MXene/CNT film sensors were carried out. MXene/CNT film sensor can keep good response and response consistency for a long time. As a novel sensor, the MXene/CNT film sensor has the advantages of high response sensitivity, solid real-time performance, and long service time. The MXene/CNT film sensor has great potential to establish and optimize manufacturing processes and to improve the cure quality of fiber-based resin composites. This sensor can be used to follow the entire life cycle of a composite from fabrication till end-of-life. (c) 2021 Elsevier B.V. All rights reserved.

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