Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 86, Issue 22, Pages 16084-16094Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.1c01688
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Funding
- CSIR
- SERB, DST, India [CRG/2020/006021]
- IISER Kolkata
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The mild and efficient electrochemically driven synthetic route allows for the access of polysubstituted selenofuran derivatives through diselenide-promoted cyclization of homopropargyl alcohols, with up to 84% isolated yield. This methodology demonstrates good functional group compatibility and further conversion to valuable furan derivatives.
The current method represents an electrochemi-cally driven synthetic route to access polysubstituted selenofuran derivatives through the diselenide-promoted cyclization of homopropargyl alcohols. The tandem electro-oxidative trans-formation operates at ambient temperature and in the absence of an external oxidant. This mild and efficient methodology exhibits good functional group compatibility, providing a broad range of substrate scopes up to 84% isolated yield. Further conversion of the seleno-functionality afforded other valuable furan derivatives.
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