4.7 Article

Theory of frequency-selective homonuclear dipolar recoupling in solid-state NMR

Related references

Note: Only part of the references are listed.
Review Chemistry, Analytical

Solid-state NMR spectroscopy in pharmaceutical sciences

Mingyue Li et al.

Summary: Solid-state NMR spectroscopy provides unique and comprehensive perspectives for analyzing pharmaceutical materials, offering insights into physiochemical stability and structural attributes of drug substances and products.

TRAC-TRENDS IN ANALYTICAL CHEMISTRY (2021)

Article Biochemistry & Molecular Biology

Spectral editing of alanine, serine, and threonine in uniformly labeled proteins based on frequency-selective homonuclear recoupling in solid-state NMR

Hang Xiao et al.

Summary: Spectral editing is essential for simplifying crowded solid-state NMR spectra of proteins. New techniques utilizing selective C-13 alpha-C-13 beta double-quantum filtering show promise in efficiently selecting signals of specific amino acid residues. These methods have the potential to streamline spectral analyses in biological solid-state NMR.

JOURNAL OF BIOMOLECULAR NMR (2021)

Article Biochemical Research Methods

Selective 1H-1H recoupling via symmetry sequences in fully protonated samples at fast magic angle spinning

Lokeswara Rao Potnuru et al.

Summary: Proton-detected solid-state NMR at fast Magic Angle Spinning (MAS) is commonly used for structural characterization of molecules using dipolar couplings. Selective proton recoupling techniques have emerged for structural characterization through estimation of qualitative and quantitative distances. The study demonstrates that well-characterized CNnv sequences can be tailored for selective recoupling of proton spins. The C6(4)(1) recoupling sequence with a modified POST-element shows selective polarization transfer efficiencies between various proton spin pairs.

JOURNAL OF MAGNETIC RESONANCE (2021)

Article Chemistry, Physical

Pulsed Third-Spin-Assisted Recoupling NMR for Obtaining Long-Range 13C-13C and 15N-13C Distance Restraints

Martin D. Gelenter et al.

JOURNAL OF PHYSICAL CHEMISTRY B (2020)

Article Chemistry, Physical

Accuracy of 1H-1H distances measured using frequency selective recoupling and fast magic-angle spinning

Lokeswara Rao Potnuru et al.

JOURNAL OF CHEMICAL PHYSICS (2020)

Article Chemistry, Physical

Selectively Enhanced 1H-1H Correlations in Proton-Detected Solid-State NMR under Ultrafast MAS Conditions

Zhengfeng Zhang et al.

JOURNAL OF PHYSICAL CHEMISTRY LETTERS (2020)

Article Chemistry, Physical

Optimization of band-selective homonuclear dipolar recoupling in solid-state NMR by a numerical phase search

Zhengfeng Zhang et al.

JOURNAL OF CHEMICAL PHYSICS (2019)

Article Chemistry, Physical

Quantitative 1H-1H Distances in Protonated Solids by Frequency-Selective Recoupling at Fast Magic Angle Spinning NMR

Nghia Tuan Duong et al.

JOURNAL OF PHYSICAL CHEMISTRY LETTERS (2018)

Article Chemistry, Physical

Selective 1H-1H Distance Restraints in Fully Protonated Proteins by Very Fast Magic-Angle Spinning Solid-State NMR

Mukul G. Jain et al.

JOURNAL OF PHYSICAL CHEMISTRY LETTERS (2017)

Article Biochemical Research Methods

Phase cycling schemes for finite-pulse-RFDR MAS solid state NMR experiments

Rongchun Zhang et al.

JOURNAL OF MAGNETIC RESONANCE (2015)

Article Biochemical Research Methods

3D 15N/15N/1H chemical shift correlation experiment utilizing an RFDR-based 1H/1H mixing period at 100 kHz MAS

Yusuke Nishiyama et al.

JOURNAL OF MAGNETIC RESONANCE (2014)

Article Biochemical Research Methods

Homonuclear dipolar recoupling under ultra-fast magic-angle spinning: Probing 19F-19F proximities by solid-state NMR

Qiang Wang et al.

JOURNAL OF MAGNETIC RESONANCE (2010)

Article Chemistry, Physical

Improved magnetization transfer in solid-state NMR with fast magic angle spinning

Markus Weingarth et al.

CHEMICAL PHYSICS LETTERS (2009)

Article Chemistry, Physical

Dipolar truncation in magic-angle spinning NMR recoupling experiments

Marvin J. Bayro et al.

JOURNAL OF CHEMICAL PHYSICS (2009)

Article Chemistry, Physical

MIRROR recoupling and its application to spin diffusion under fast magic-angle spinning

Ingo Scholz et al.

CHEMICAL PHYSICS LETTERS (2008)

Review Chemistry, Physical

Proton assisted recoupling and protein structure determination

Gael De Paepe et al.

JOURNAL OF CHEMICAL PHYSICS (2008)

Article Chemistry, Multidisciplinary

Solid-State Protein-Structure Determination with Proton-Detected Triple-Resonance 3D Magic-Angle-Spinning NMR Spectroscopy

Donghua H. Zhou et al.

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION (2007)

Article Chemistry, Physical

Frequency-selective homonuclear dipolar recoupling in solid state NMR

Anant K. Paravastu et al.

JOURNAL OF CHEMICAL PHYSICS (2006)

Article Chemistry, Physical

Broadband rotational resonance in solid state NMR spectroscopy

JCC Chan et al.

JOURNAL OF CHEMICAL PHYSICS (2004)

Article Chemistry, Multidisciplinary

13C-13C rotational resonance width distance measurements in uniformly 13C-labeled peptides

R Ramachandran et al.

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY (2003)

Article Chemistry, Physical

Band-selective homonuclear dipolar recoupling in rotating solids

M Hohwy et al.

JOURNAL OF CHEMICAL PHYSICS (2002)

Article Biochemical Research Methods

Double-quantum dipolar recoupling at high magic-angle spinning rates

PE Kristiansen et al.

JOURNAL OF MAGNETIC RESONANCE (2002)

Article Biochemical Research Methods

Homonuclear zero-quantum recoupling in fast magic-angle spinning nuclear magnetic resonance

A Brinkmann et al.

JOURNAL OF MAGNETIC RESONANCE (2002)

Article Biochemical Research Methods

SIMPSON: A general simulation program for solid-state NMR spectroscopy

M Bak et al.

JOURNAL OF MAGNETIC RESONANCE (2000)

Article Biochemical Research Methods

Spinning-frequency-dependent narrowband RF-driven dipolar recoupling

G Goobes et al.

JOURNAL OF MAGNETIC RESONANCE (2000)

Article Biochemical Research Methods

Sensitivity enhancement in solid state N-15 NMR by indirect detection with high-speed magic angle spinning

Y Ishii et al.

JOURNAL OF MAGNETIC RESONANCE (2000)

Article Biochemical Research Methods

An improved broadband decoupling sequence for liquid crystals and solids

BM Fung et al.

JOURNAL OF MAGNETIC RESONANCE (2000)