Journal
JOURNAL OF APPLIED POLYMER SCIENCE
Volume 139, Issue 22, Pages -Publisher
WILEY
DOI: 10.1002/app.52260
Keywords
dicyandiamide; epoxy resin; oil well repairing
Categories
Funding
- National Natural Science Foundation of China [51874210]
- China Postdoctoral Science Foundation [2020TQ0221, 2021M692391]
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By adding bisphenol F epoxy resin, dicyandiamide hardener, and urea accelerator, an epoxy resin system has been developed to prevent casing-casing annulus pressure. The system meets the requirements of on-site construction with initial consistency less than 30 Bc, thickening time of 3-4 hours, and compressive strength above 27 MPa at 90 degrees C.
In the development of unconventional oil and gas resources, such as offshore oil, high pressure oil and sour wells, casing-casing annulus pressure is a common problem. To prevent casing-casing annulus pressure, bisphenol F epoxy resin, dicyandiamide hardener SH-500A and urea accelerator SH-A100 are added to develop an epoxy resin system. The thickening time and the compressive strength at 90 degrees C are used as the main evaluation indexes. The optimal formulation was found to be as follows: bisphenol F epoxy resin NPEF-170 with 20 wt% of diluent benzyl glycidyl ether, 9.0 wt% of hardener dicyandiamide and 0.5-0.4 wt% of urea accelerator SH-A100. The experimental results showed that the initial consistency of the epoxy resin system is less than 30 Bc, the thickening time is 3-4 h, and the compressive strength at 90 degrees C is above 27 MPa, which meet the requirements of on-site construction.
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