4.7 Article

The evolution of microstructure and mechanical properties of Zn-0.8Mg-0.2Sr alloy prepared by casting and extrusion

Journal

JOURNAL OF ALLOYS AND COMPOUNDS
Volume 906, Issue -, Pages -

Publisher

ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2022.164308

Keywords

Zinc; Magnesium; Biodegradable; Microstructure; Mechanical properties; Texture

Funding

  1. Czech Science Foundation [18-06110S]
  2. Operational Programme Research, Development and Education - European Structural and Investment Funds [SOLID21 -CZ.02.1.01/0.0/0.0/16_019/0000760]
  3. Czech Ministry of Education, Youth and Sports [SOLID21 -CZ.02.1.01/0.0/0.0/16_019/0000760, LM2018110]
  4. Ministry of Education, Science, Research and Sport of the Slovak Republic [1/0531/22]
  5. [SOLID21-CZ.02.1.01/0.0/0.0/16_019/0000760]

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This paper investigates the effects of extrusion temperature and ratio on the microstructure and mechanical properties of Zn-0.8Mg-0.2Sr alloy. The results show that the grain size, material texture, and dislocation substructures have a significant influence on the alloy's elongation range and anisotropy. Under appropriate extrusion conditions, the alloy's mechanical properties can be greatly improved.
Zinc-based alloys containing elements well-tolerated by the organism (Mg, Ca, Sr) are considered as perspective biodegradable materials for an application like medical devices such as fixations of fractured bones or even stents. In the presented paper we characterize the relations between microstructure and mechanical properties of extruded Zn-0.8Mg-0.2 Sr alloy (wt%) depending on various parameters like extrusion temperature (150-300 degrees C) and ratio (11 or 25). Typical analysis including SEM with EBSD and mechanical tests indicate a strong dependence of obtained data on both extrusion temperature and ratio. Relatively wide range of elongation to fracture (2-22%) and anisotropy in compression yield strengths regarding loading direction (50-150 MPa) are explained by the huge effect of grain size, material texture and also the existence of dislocation substructures in materials extruded at elevated temperatures. Based on obtained results, appropriate extrusion conditions (200 degrees C, extrusion ratio 25) are suggested to reach the combination of superior mechanical properties 244 MPa, 324 MPa and 22% for tensile yield strength, ultimate tensile strength and elongation to fracture, respectively.(c) 2022 Published by Elsevier B.V.

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