Physicochemical properties and digestion mechanism of starch-linoleic acid complex induced by multi-frequency power ultrasound

The effects of multi-frequencies (mono: 20 kHz, 40 kHz, 60 kHz; dual: 20/40 kHz, 40/60 kHz, 20/60 kHz, and tri: 20/40/60 kHz) on physicochemical properties and in vitro digestibility of arrowhead starch-linoleic acid (AS-LA) complexes were evaluated. The complexing index and FTIR analyses showed that sonication treatment might be helpful in the formation of AS-LA complexes in an ultrasound frequency-dependent manner. The SEM micrographs revealed that the various ultrasonication frequencies caused dense network structure in AS-LA complexes. The XRD showed a V-type crystalline structure with increased crystallinity. Compared with arrowhead starch, a decrease in rapidly digestible starch , and an increase in resistant starch contents of AS-LA under various ultrasound frequencies was due to arrowhead starch and linoleic acid molecular interactions, which inhibited the further binding abilities. As a non-thermal technology, ultrasound could be effectively employed to prepare starch-lipid complexes with significant potential in functional foods and drug delivery systems.

Automated summary

The effects of ultrasound treatment at different frequencies on the physicochemical properties and digestibility of arrowhead starch-linoleic acid complexes were studied. The results showed that ultrasound treatment influenced the formation of the complexes, resulting in changes in network structure and crystallinity. Ultrasound was found to be a non-thermal technology that can be effectively used to prepare starch-lipid complexes with potential functional applications.