4.6 Article

Effect of post-curing light exposure time on the physico-mechanical properties and cytotoxicity of 3D-printed denture base material

Journal

DENTAL MATERIALS
Volume 38, Issue 1, Pages 57-67

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.dental.2021.10.011

Keywords

3D printed denture base materials; Flexural strength; Fracture toughness; Vickers hardness; Degree of conversion; Cytotoxicity

Funding

  1. Faculty of Health and Medical Sciences, Dental School University of Western Australia
  2. Australian Dental Research Foundation [PG 00800/51002200, 00800/51001600]
  3. Colgate Palmolive(R) [PG 008/10402012, 00800/70237003, 00800/68001004]

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This study investigated the effect of post curing light exposure time on the physico-mechanical properties and cytotoxicity of a 3D-printed PMMA-based denture material. The results showed that the flexural strength, toughness, and surface hardness of the material significantly improved with longer post curing time, and the cell viability also increased.
Objective: This study investigated the effect of post curing light exposure time on the physico-mechanical properties and cytotoxicity of a 3D-printed PMMA-based denture ma-terial in comparison to a conventional heat-cured alternative as a control. Methods: 3D-printed specimens were fabricated followed by post-curing for 0, 5, 10 or 20 min at 200 W and light wavelength range of 390-540 nm. Heat-cured specimens were fabricated using a standard protocol. Specimens were placed in artificial saliva at 37 celcius for 48 h (immediate groups) and 6 months (aged group), then evaluated flexural strength/ modulus, fracture toughness, microhardness, and degree of conversion. Water sorption and solubility was assessed after 28 days. Flexural strength, flexural modulus, and fracture toughness were tested through three-point bending tests, while the surface hardness was tested using Vickers's test. Fractured specimens were viewed by scanning electron mi-croscope (SEM). Cytotoxicity in term of cell viability was evaluated using human oral fi-broblasts. Results: Flexural strength/modulus, fracture toughness and surface hardness significantly improved with the increase in light curing time up to 20 min. The same pattern of im-provement was found with degree of conversion, water sorption, solubility, and cell via-bility. There was no significant difference (p < 0.01) between heat-cured material and 3D specimens post-cured for 20 min in term of flexural strength/modulus, surface hardness, and degree of conversion at the two-storage time points. Significance: Generally, the physico-mechanical properties of the 3D-printed denture base material improve as post curing time increases up to 20 min which exhibited comparable performance as the conventional heat-cured control. (c) 2021 The Academy of Dental Materials. Published by Elsevier Inc. All rights reserved.

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