Journal
CHEMICAL COMMUNICATIONS
Volume 58, Issue 16, Pages 2670-2673Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d2cc00374k
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Funding
- National Natural Science Foundation of China [21773021]
- Fundamental Research Funds for the Central Universities [DUT20ZD217]
- LiaoNing Revitalization Talents Program [XLYC1802030]
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This paper describes an unprecedented three-component addition reaction, which allows for the efficient synthesis of gem-dichloroalkane derivatives in mild conditions without affecting important functional groups.
This paper described the unprecedented three-component addition of terminal alkynes, carboxylic acids, and tert-butyl hypochlorite. This new type of addition proceeds smoothly to produce gem-dichloroalkane derivatives in satisfactory to excellent yields via successive two-time additions under mild conditions. The synthetically useful functional groups, such as Cl, Br, CN, and NO2, remained intact in the final products.
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