4.7 Article

Rapid synthesis of Y3Al5O12 powders via plasma electrolysis

Journal

CERAMICS INTERNATIONAL
Volume 47, Issue 21, Pages 30147-30155

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2021.07.193

Keywords

Plasma electrolysis; Composite oxide ceramic powder; Yttrium aluminum garnet (Y3Al5O12 YAG)

Funding

  1. Basic Research Plan from Beijing Institute of Technology [201920941008]
  2. Key Research and Development Project of Guangdong Provincefrom China [2019B090908004]

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This study aimed to rapidly synthesize Y3Al5O12 using plasma electrolysis for the first time, and studied the topography, structure, and elements of the prepared powder through SEM and XRD. The results showed that the synthesized Y3Al5O12 powder had a good crystal form and high purity.
Yttrium aluminum garnet (Y3Al5O12, YAG) is an important functional material. However, the strict and complicated preparation has limited its wide application. This study aimed to rapidly synthesize Y3Al5O12 by plasma electrolysis for the first time. The prepared powder was studied from topography, structure and elements by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The powder had a good crystal form with a spherical shape. The single kind of diffraction peak of Y3Al5O12 in XRD revealed the high purity of the synthesized powders. The study of the relationship between the applied voltage and the synthesized powder revealed a threshold voltage of 210 V under the present condition. The higher voltage led to the damage of the electrode due to excessive heat. The synthesis of the YAG powder had a melt-quench process. The two processes were carried out at the same time.

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